High performance anion exchange chromatography with pulsed amperometric detection for simultaneous determination of monosaccharides and uronic acids
文献类型：期刊论文
| 作者 | Liang Li'na; Zhang Ping; Cai Yaqi; Mou Shifen |
| 刊名 | CHINESE JOURNAL OF ANALYTICAL CHEMISTRY
 |
| 出版日期 | 2006 |
| 卷号 | 34期号:10页码:1371-1374 |
| 关键词 | monosaccharide uronic acid high performance anion exchange chromatography pulsed amperometric detection |
| 英文摘要 | A method for determination of eight monosacchanides and two uronic acids in polysaccharide and wood hemicellulose hydrolysate by high performance anion exchange chromatography with pulsed amperometric detection was established. The chromatographic separation was established on a Dionex CarboPac PA20 anion exchange column using NaOH and NaAc gradient elution (50 similar to 200 mmol/L) at 0. 5 mL/min flow rate. The total analysis time is 30 min. Detection limits of 2.5 - 14.4 mu g/L (25 mu L injection) were achieved under the optimized conditions. RSDs of the peak area for the seven consecutive determinations of 5 mg/L eight monosaccharides and two uronic acids were 0.3% - 1.5%. The method had been applied for determination of eight monosaccharides and two uronic acids in,hydrolysates of polysacchanide and wood hemicellulose. |
| WOS记录号 | WOS:000243502600003 |
| 源URL | [http://ir.rcees.ac.cn/handle/311016/22884]  |
| 专题 | 生态环境研究中心_环境化学与生态毒理学国家重点实验室 |
| 推荐引用方式 GB/T 7714 | Liang Li'na,Zhang Ping,Cai Yaqi,et al. High performance anion exchange chromatography with pulsed amperometric detection for simultaneous determination of monosaccharides and uronic acids[J]. CHINESE JOURNAL OF ANALYTICAL CHEMISTRY,2006,34(10):1371-1374. |
| APA | Liang Li'na,Zhang Ping,Cai Yaqi,&Mou Shifen.(2006).High performance anion exchange chromatography with pulsed amperometric detection for simultaneous determination of monosaccharides and uronic acids.CHINESE JOURNAL OF ANALYTICAL CHEMISTRY,34(10),1371-1374. |
| MLA | Liang Li'na,et al."High performance anion exchange chromatography with pulsed amperometric detection for simultaneous determination of monosaccharides and uronic acids".CHINESE JOURNAL OF ANALYTICAL CHEMISTRY 34.10(2006):1371-1374. |
入库方式： OAI收割
来源：生态环境研究中心
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