Electrochemical preparation of composite polyaniline coating and its application in the determination of bisphenol A, 4-n-nonylphenol, 4-tert-octyl phenol using direct solid phase microextraction coupled with high performance liquid chromatography
文献类型:期刊论文
作者 | Huang, MJ; Jiang, GB; Cai, YQ |
刊名 | JOURNAL OF SEPARATION SCIENCE
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出版日期 | 2005 |
卷号 | 28期号:16页码:2218-2224 |
关键词 | composite polyaniline (CPANI) electroplating method fiber preparation metal wires solid phase microextraction |
英文摘要 | For SPME-HPLC, metal wires with better mechanical strength are preferred over the fused silica fibers. In this article, a novel composite polyaniline (CPANI) doped with PEG and polydimethylsiloxane coating (CPANI fiber) was prepared on a stainless steel wire by a three-electrode system: the fiber was used as the work electrode, a calomel electrode and a platinum electrode were used as the reference and the counter electrodes, respectively. To evaluate the new CPANI coating, the coating was used to extract three kinds of phenols (bisphenol A, 4-n-nonylphenol, and 4-tert-octylphenol) in water samples by direct-SPME mode and then desorbed in commercial SPME-HPLC interface to separation. The extraction procedure was also optimized. Five real water samples were investigated. Good recoveries were gained when environmental samples were analyzed. |
学科主题 | Chemistry |
研究领域[WOS] | Chemistry |
WOS记录号 | WOS:000233398800024 |
源URL | [http://ir.rcees.ac.cn/handle/311016/23177] ![]() |
专题 | 生态环境研究中心_环境化学与生态毒理学国家重点实验室 |
推荐引用方式 GB/T 7714 | Huang, MJ,Jiang, GB,Cai, YQ. Electrochemical preparation of composite polyaniline coating and its application in the determination of bisphenol A, 4-n-nonylphenol, 4-tert-octyl phenol using direct solid phase microextraction coupled with high performance liquid chromatography[J]. JOURNAL OF SEPARATION SCIENCE,2005,28(16):2218-2224. |
APA | Huang, MJ,Jiang, GB,&Cai, YQ.(2005).Electrochemical preparation of composite polyaniline coating and its application in the determination of bisphenol A, 4-n-nonylphenol, 4-tert-octyl phenol using direct solid phase microextraction coupled with high performance liquid chromatography.JOURNAL OF SEPARATION SCIENCE,28(16),2218-2224. |
MLA | Huang, MJ,et al."Electrochemical preparation of composite polyaniline coating and its application in the determination of bisphenol A, 4-n-nonylphenol, 4-tert-octyl phenol using direct solid phase microextraction coupled with high performance liquid chromatography".JOURNAL OF SEPARATION SCIENCE 28.16(2005):2218-2224. |
入库方式: OAI收割
来源:生态环境研究中心
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