中国科学院机构知识库网格
Chinese Academy of Sciences Institutional Repositories Grid
Analytical method for trace send-volatile organic compounds in the soil of Beijing suburbs

文献类型:期刊论文

作者Ma, LL; Lao, WJ; Wang, XT; Liu, H; Chu, SG; Xu, XB
刊名CHINESE JOURNAL OF ANALYTICAL CHEMISTRY
出版日期2003
卷号31期号:9页码:1025-1029
关键词Semi-volatile organic compounds soil analysis
英文摘要We developed a method for the determination of trace semi-volatile organic compounds (SVOC) in soil by ultrasonic extraction, column separation and gas chromatography-mass spectrometry (GC-MS). The conditions for separation of SVOC adsorbed by silica gel or Florisil columns were optimized. The average recovery was 82% similar to 105% for n-alkanes, 103% similar to 110% for polycyclic aromatic hydrocarbons (PAHs), 94% similar to 117% for organochlorine pesticides (OCPs) and 86% similar to 114% for phthalate esters (PAEs). The limit of detection was 3 22, 3 similar to 42, 0.004 similar to 0.088 and 10 similar to 220 ng/g for n-alkanes, PAHs, OCPs and PAEs, respectively. The relative standard deviations (RSD) were all below 15%. The method was used for the analysis of SVOC in soil samples in the Beijing suburban areas. The results of quality control showed that the method allowed the reliable investigation.
研究领域[WOS]Chemistry
WOS记录号WOS:000185756200001
源URL[http://ir.rcees.ac.cn/handle/311016/23666]  
专题生态环境研究中心_环境化学与生态毒理学国家重点实验室
推荐引用方式
GB/T 7714
Ma, LL,Lao, WJ,Wang, XT,et al. Analytical method for trace send-volatile organic compounds in the soil of Beijing suburbs[J]. CHINESE JOURNAL OF ANALYTICAL CHEMISTRY,2003,31(9):1025-1029.
APA Ma, LL,Lao, WJ,Wang, XT,Liu, H,Chu, SG,&Xu, XB.(2003).Analytical method for trace send-volatile organic compounds in the soil of Beijing suburbs.CHINESE JOURNAL OF ANALYTICAL CHEMISTRY,31(9),1025-1029.
MLA Ma, LL,et al."Analytical method for trace send-volatile organic compounds in the soil of Beijing suburbs".CHINESE JOURNAL OF ANALYTICAL CHEMISTRY 31.9(2003):1025-1029.

入库方式: OAI收割

来源:生态环境研究中心

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