Determination of PCBs in tetrachlorinated quinone using gas chromatography with electron capture detection
文献类型：期刊论文
| 作者 | Bi, XH; Xu, XB; Zheng, MH; Meng, QY; Fu, S |
| 刊名 | TALANTA
 |
| 出版日期 | 2000 |
| 卷号 | 52期号:3页码:397-402 |
| 关键词 | PCBs 2 gas chromatography 3 5 6-tetrachloro-1 4-benzoquinone |
| 英文摘要 | A simple, sensitive method for determining polychlorinated biphenyl (PCB) congeners in industrial product 2,3,5.6-tetrachloro-1,4-benzoquinone with GC/ECD detection has been developed. The method based on liquid-liquid extraction from tetrachlorinated quinone dissolved in N,N-dimethylformamide was found to be efficient for the determination of the levels of the investigated pollutants. A series of extraction and purification steps were designed for the sample pretreatment. The congener specific averages of recoveries were 82-96% for Aroclor 1242 and 1254 at a total spiking level of ca. 0.4 mu g g(-1) sample. The reproducibilities of replicate determinations of different congeners were typically 5-19% except one with the average 13% R.S.D. (n = 3). This method was applied to evaluate the background levels of PCBs in tetrachloro-1,4-benzoquinone, of which the corresponding PCB levels varied from 0.014 to 1.5 mu g g(-1). (C) 2000 Elsevier Science B.V. All rights reserved. |
| WOS记录号 | WOS:000087888400003 |
| 源URL | [http://ir.rcees.ac.cn/handle/311016/24136]  |
| 专题 | 生态环境研究中心_环境化学与生态毒理学国家重点实验室 |
| 推荐引用方式 GB/T 7714 | Bi, XH,Xu, XB,Zheng, MH,et al. Determination of PCBs in tetrachlorinated quinone using gas chromatography with electron capture detection[J]. TALANTA,2000,52(3):397-402. |
| APA | Bi, XH,Xu, XB,Zheng, MH,Meng, QY,&Fu, S.(2000).Determination of PCBs in tetrachlorinated quinone using gas chromatography with electron capture detection.TALANTA,52(3),397-402. |
| MLA | Bi, XH,et al."Determination of PCBs in tetrachlorinated quinone using gas chromatography with electron capture detection".TALANTA 52.3(2000):397-402. |
入库方式： OAI收割
来源：生态环境研究中心
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