Determination of benzoyl peroxide in wheat flour by ion chromatography with precolumn derivatization
文献类型：期刊论文
| 作者 | Chen, QC; Mou, SF; Hou, XP; Ni, ZM |
| 刊名 | JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES
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| 出版日期 | 1998 |
| 卷号 | 21期号:5页码:705-716 |
| 英文摘要 | A novel method for the determination of benzoyl peroxide bleach in wheat flour by using high performance anion exchange chromatography (HPIC) after decomposition to benzoic acid was proposed. Benzoyl peroxide was effectively extracted from wheat flour with absolute ethanol by ultrasonication under neutral condition and converted to benzoic acid in the presence of potassium hydroxide solution. The chromatographic separation of benzoic acid was performed on a Dionex OmniPac PAX-100 separation column and the determination by ultraviolet absorbance detection at 222 nm. Good linearity between the concentration of benzoyl peroxide and peak area response nas achieved in the range of 0.12-20 mu g/mL. The detection limit (signal-to-noise ratio 3:1) was 19 ng/mL for benzoyl peroxide. The method has been successfully applied for the analysis of real samples, and the average recoveries for various samples ranged from 81 to 92%. |
| 研究领域[WOS] | Biochemistry & Molecular Biology ; Chemistry |
| WOS记录号 | WOS:000072927700008 |
| 源URL | [http://ir.rcees.ac.cn/handle/311016/24287]  |
| 专题 | 生态环境研究中心_环境化学与生态毒理学国家重点实验室 |
| 推荐引用方式 GB/T 7714 | Chen, QC,Mou, SF,Hou, XP,et al. Determination of benzoyl peroxide in wheat flour by ion chromatography with precolumn derivatization[J]. JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES,1998,21(5):705-716. |
| APA | Chen, QC,Mou, SF,Hou, XP,&Ni, ZM.(1998).Determination of benzoyl peroxide in wheat flour by ion chromatography with precolumn derivatization.JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES,21(5),705-716. |
| MLA | Chen, QC,et al."Determination of benzoyl peroxide in wheat flour by ion chromatography with precolumn derivatization".JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES 21.5(1998):705-716. |
入库方式： OAI收割
来源：生态环境研究中心
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