Microwave synthesis of AFI-type aluminophosphate molecular sieve under solvent-free conditions
文献类型：期刊论文
| 作者 | Zhao XH(赵新红)1; Zhao, Jiangbo1; Wen, Juanjuan1; Li A(李安)1; Li GX(李贵贤)1; Wang XL(王晓来)2
|
| 刊名 | Microporous and Mesoporous Materials
 |
| 出版日期 | 2015 |
| 卷号 | 213页码:192-196 |
| ISSN号 | 1387-1811 |
| 关键词 | AlPO4-5 Solvent-free Hierarchical porous Microwave |
| 通讯作者 | 赵新红 |
| 英文摘要 | AlPO4-5 aluminophosphate molecular sieve with AFI topology has been successfully synthesized by microwave irradiation under solvent-free conditions. The key influential factors controlling the crystallization of AFI structure were thoroughly investigated. The optimum synthetic conditions of this material are as follows: the initial composition is 1.0Al2O3: 3.0P2O5: 2.0HF: 8.0TEABr(tetraethylammonium bromide): 125C, aluminum isopropoxide is the best aluminum source, and activated carbon needs to be pretreated before used as the reaction medium and hard template. The resultant AlPO4-5 molecular sieves were characterized by X-ray diffraction (XRD), N2 physisorption, scanning electron microscopy (SEM) and transmission electron microscopy (TEM). The results reveal that the obtained samples exhibit hierarchically porous characteristic. |
| 学科主题 | 物理化学与绿色催化 |
| 资助信息 | the National Natural Science Foundation of China (Grant No. 21306072;51263012);Development Program of Lanzhou University of Technology for excellent teachers (Grant No. Q201113) |
| 收录类别 | SCI |
| 语种 | 英语 |
| WOS记录号 | WOS:000356186900024 |
| 源URL | [http://210.77.64.217/handle/362003/18337]  |
| 专题 | 兰州化学物理研究所_OSSO国家重点实验室 |
| 作者单位 | 1.Lanzhou Univ Technol, Sch Petrochem Engn, Lanzhou 730050, Peoples R China 2.Chinese Acad Sci, Lanzhou Inst Chem Phys, State Key Lab Oxo Synth & Select Oxidat, Lanzhou 730000, Peoples R China |
| 推荐引用方式 GB/T 7714 | Zhao XH,Zhao, Jiangbo,Wen, Juanjuan,et al. Microwave synthesis of AFI-type aluminophosphate molecular sieve under solvent-free conditions[J]. Microporous and Mesoporous Materials,2015,213:192-196. |
| APA | Zhao XH,Zhao, Jiangbo,Wen, Juanjuan,Li A,Li GX,&Wang XL.(2015).Microwave synthesis of AFI-type aluminophosphate molecular sieve under solvent-free conditions.Microporous and Mesoporous Materials,213,192-196. |
| MLA | Zhao XH,et al."Microwave synthesis of AFI-type aluminophosphate molecular sieve under solvent-free conditions".Microporous and Mesoporous Materials 213(2015):192-196. |
入库方式： OAI收割
来源：兰州化学物理研究所
浏览0
下载0
收藏0
其他版本
除非特别说明，本系统中所有内容都受版权保护，并保留所有权利。