A NOVEL RHEIN-FUNCTIONALIZED RESIN WITH APPLICATION FOR THE PRECONCENTRATION OF ANTHRAQUINONES
文献类型：期刊论文
| 作者 | Xie, Jing ; Liao, Xun ; Qing, Fang-Zhu ; Luo, Pei ; Zhang, Zhi-Feng ; Huang, Jing ; Qing, Lin-Sen |
| 刊名 | ANALYTICAL LETTERS
 |
| 出版日期 | 2014 |
| 卷号 | 47期号:14页码:2332-2340 |
| 关键词 | Anthraquinone High-performance liquid chromatography-tandem mass spectrometry Polygonum cuspidatum Rhein Sample preparation Solid-phase extraction |
| 产权排序 | 2 |
| 通讯作者 | Huang, J (reprint author), Sichuan Univ, Chengdu 610041, Peoples R China. |
| 合作状况 | 其它 |
| 英文摘要 | Anthraquinones are active components of herbal medicine, and consequently it is necessary to develop a selective, convenient, and green preconcentration method for these compounds. A rhein-functionalized resin was synthesized by a condensation reaction followed by characterization by infrared spectroscopy, transmission electron microscopy, solid carbon-13 nuclear magnetic resonance, and elemental analysis. The rhein-functionalized resin was employed for solid-phase extraction with HPLC-MS for the determination of anthraquinones in the extracts of Polygonum cuspidatum. Emodin, chrysophanol, and physcion were selectively concentrated by a simple absorption and desorption procedure. The results indicated that this new material has application for separating and enriching anthraquinones from herbal medicine, which is significant for pharmaceutical analysis. |
| 学科主题 | Chemistry, Analytical |
| 收录类别 | SCI |
| 语种 | 英语 |
| 公开日期 | 2016-02-26 |
| 源URL | [http://210.75.237.14/handle/351003/26702]  |
| 专题 | 成都生物研究所_天然产物研究 |
| 推荐引用方式 GB/T 7714 | Xie, Jing,Liao, Xun,Qing, Fang-Zhu,et al. A NOVEL RHEIN-FUNCTIONALIZED RESIN WITH APPLICATION FOR THE PRECONCENTRATION OF ANTHRAQUINONES[J]. ANALYTICAL LETTERS,2014,47(14):2332-2340. |
| APA | Xie, Jing.,Liao, Xun.,Qing, Fang-Zhu.,Luo, Pei.,Zhang, Zhi-Feng.,...&Qing, Lin-Sen.(2014).A NOVEL RHEIN-FUNCTIONALIZED RESIN WITH APPLICATION FOR THE PRECONCENTRATION OF ANTHRAQUINONES.ANALYTICAL LETTERS,47(14),2332-2340. |
| MLA | Xie, Jing,et al."A NOVEL RHEIN-FUNCTIONALIZED RESIN WITH APPLICATION FOR THE PRECONCENTRATION OF ANTHRAQUINONES".ANALYTICAL LETTERS 47.14(2014):2332-2340. |
入库方式： OAI收割
来源：成都生物研究所
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