Determination of impurities in titanium nitride by slurry introduction axial viewed inductively coupled plasma optical emission spectrometry
文献类型：会议论文
| 作者 | Wang, Z; Ni, ZM; Qui, DR; Tao, GY; Yang, PY |
| 出版日期 | 2005 |
| 会议名称 | 6th European Furnace Symposium/11th Solid Sampling Colloquium |
| 会议日期 | JUN 27-30, 2004 |
| 会议地点 | Balatonfoldvar, HUNGARY |
| 关键词 | slurry TiN axial ICP-OES NH(4)PAA intrinsic internal standard |
| 英文摘要 | A method of slurry nebulization for inductively coupled plasma optical emission spectrometry (ICP-OES) applied to the analysis of titanium niride(TiN) was reported. The TiN slurry sample was prepared with adding dispersant polyacrylate amine or polyethylene imine for the stabilization and homogenization of suspension, and the amount of additives was optimized. A Babington type cross-flow nebulizer with V-groove was used for nebulization of the slurry for avoidance of blockage from the particles. The stability of slun-y was characterized via zeta potential measurement, scanning electron microscope observation, particle size distrbution measurement and signal stability testing. For nm size TiN, calibration curves could be established by aqueous standards and the analytical results were in good accordance with the alkaline fusion method. For μ m size TiN, a negative deviation was observed for most of elements and this deviation can be corrected by using Ti intrinsic internal standard method. © 2005 Elsevier B.V. All rights reserved. |
| ISSN号 | 0584-8547 |
| 源URL | [http://ir.rcees.ac.cn/handle/311016/24764]  |
| 专题 | 生态环境研究中心_环境化学与生态毒理学国家重点实验室 |
| 推荐引用方式 GB/T 7714 | Wang, Z,Ni, ZM,Qui, DR,et al. Determination of impurities in titanium nitride by slurry introduction axial viewed inductively coupled plasma optical emission spectrometry[C]. 见:6th European Furnace Symposium/11th Solid Sampling Colloquium. Balatonfoldvar, HUNGARY. JUN 27-30, 2004. |
入库方式： OAI收割
来源：生态环境研究中心
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