Characterization and photocatalytic activity of transition-metal-supported surface bond-conjugated TiO2/SiO2
文献类型：会议论文
| 作者 | Chun, H; Tang, YC; Tang, HX |
| 出版日期 | 2004 |
| 会议名称 | 16th International Ion Chromography Symposium |
| 会议日期 | SEP 21-24, 2003 |
| 会议地点 | San Diego, CA |
| 关键词 | detection waveforms pulsed amperometric detection neomycin antibiotics aminoglycosides glycosidcs LC |
| 英文摘要 | Determination of neomycin is important for quality control of the pharmaceutical preparation. A quadruple-potential waveform used for pulsed amperometric detection of neomycin was investigated. The waveform cleans the electrode by application of a potential more negative than the potential limit to avoid the formation of gold oxide during applying positive potential to clean gold electrode, thus decreasing the dissolution resulting recession of the gold working electrode within gold oxide formation/reduction cycles in the triple-potential waveform. Waveform parameters were optimized to maximize the signal-to-noise ratio (S/N). The detection limit of neomycin B is lower than 0.01 mug/ml. The linearity of framycetin (plotted as peak area of neomycin B) ranges from 0.05 to 100 mug/ml with correlation coefficient 0.9998. R.S.D. (it = 60) of the peak area of neomycin B is lower than 2%. The quadruple-potential waveform shows low detection limits and long-term reproducibility. (C) 2004 Elsevier B.V. All rights reserved. |
| 源URL | [http://ir.rcees.ac.cn/handle/311016/24781]  |
| 专题 | 生态环境研究中心_环境化学与生态毒理学国家重点实验室 |
| 推荐引用方式 GB/T 7714 | Chun, H,Tang, YC,Tang, HX. Characterization and photocatalytic activity of transition-metal-supported surface bond-conjugated TiO2/SiO2[C]. 见:16th International Ion Chromography Symposium. San Diego, CA. SEP 21-24, 2003. |
入库方式： OAI收割
来源：生态环境研究中心
浏览0
下载0
收藏0
其他版本
除非特别说明，本系统中所有内容都受版权保护，并保留所有权利。