Suppression of Bragg reflection glitches of a single-crystal diamond anvil cell by a polycapillary half-lens in high-pressure XAFS spectroscopy
文献类型:期刊论文
作者 | Chen DL(陈栋梁)![]() ![]() |
刊名 | JOURNAL OF SYNCHROTRON RADIATION
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出版日期 | 2013 |
卷号 | 20期号:2页码:243-248 |
关键词 | high-pressure m-XAFS DAC polycapillary half-lens optics Ge K-edge |
英文摘要 | In combination with a single-crystal diamond anvil cell (DAC), a polycapillary half-lens (PHL) re-focusing optics has been used to perform high-pressure extended X-ray absorption fine-structure measurements. It is found that a large divergent X-ray beam induced by the PHL leads the Bragg glitches from single-crystal diamond to be broadened significantly and the intensity of the glitches to be reduced strongly so that most of the DAC glitches are efficiently suppressed. The remaining glitches can be easily removed by rotating the DAC by a few degrees with respect to the X-ray beam. Accurate X-ray absorption fine-structure (XAFS) spectra of polycrystalline Ge powder with a glitch-free energy range from -200 to 800 eV relative to the Ge absorption edge are obtained using this method at high pressures up to 23.7 GPa, demonstrating the capability of PHL optics in eliminating the DAC glitches for high-pressure XAFS experiments. This approach brings new possibilities to perform XAFS measurements using a DAC up to ultrahigh pressures. |
学科主题 | Instruments & Instrumentation; Optics; Physics |
收录类别 | SCI |
WOS记录号 | WOS:000314929700006 |
公开日期 | 2016-05-03 |
源URL | [http://ir.ihep.ac.cn/handle/311005/223907] ![]() |
专题 | 高能物理研究所_多学科研究中心 |
推荐引用方式 GB/T 7714 | Chen DL,Dong JC,Zhang XL,et al. Suppression of Bragg reflection glitches of a single-crystal diamond anvil cell by a polycapillary half-lens in high-pressure XAFS spectroscopy[J]. JOURNAL OF SYNCHROTRON RADIATION,2013,20(2):243-248. |
APA | 陈栋梁.,董俊才.,张晓丽.,Chen, DL.,Dong, JC.,...&刘景.(2013).Suppression of Bragg reflection glitches of a single-crystal diamond anvil cell by a polycapillary half-lens in high-pressure XAFS spectroscopy.JOURNAL OF SYNCHROTRON RADIATION,20(2),243-248. |
MLA | 陈栋梁,et al."Suppression of Bragg reflection glitches of a single-crystal diamond anvil cell by a polycapillary half-lens in high-pressure XAFS spectroscopy".JOURNAL OF SYNCHROTRON RADIATION 20.2(2013):243-248. |
入库方式: OAI收割
来源:高能物理研究所
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