Preparative separation of nine flavonoids from Pericarpium Citri Reticulatae by preparative-HPLC and HSCCC
文献类型：期刊论文
| 作者 | Ye, Xiaolan ; Cao, Di ; Song, Fenyun ; Fan, Guorong ; Wu, Fuhai |
| 刊名 | SEPARATION SCIENCE AND TECHNOLOGY
 |
| 出版日期 | 2016 |
| 卷号 | 51期号:5页码:807-815 |
| 关键词 | POLYMETHOXYLATED FLAVONES ANTIINFLAMMATORY ACTIVITY LIQUID-CHROMATOGRAPHY IDENTIFICATION ANTICANCER CHEMISTRY APOPTOSIS EXTRACTS CELLS |
| ISSN号 | 0149-6395 |
| 中文摘要 | An economical and systematized chromatographic separation process to isolate and purify flavonoids from Pericarpium Citri Reticulatae was developed. Solvent refluxing extraction, macroporous resin column, preparative HPLC and HSCCC (high-speed counter-current chromatography) were used for extraction, fraction, isolation, and purification of nine flavonoids including vicenin-2(42 mg), hesperidin (108 mg), isosinensetin (15 mg), sinensetin (10 mg), tetramethyl-O-isoscutellarein (11 mg), nobiletin (121 mg), 3, 5, 6, 7, 8, 3 ',4 '-heptamethoxyflavone (34 mg), tangeretin (114 mg), and 5-demethylnobiletin (13 mg) from Pericarpium Citri Reticulatae, and their purities were all above 98%. All these constituents were identified by UV, MS, H-1 NMR, and C-13 NMR. The procedure and techniques described here can provide a useful reference for the preparative-scale isolation of some flavonoids in a fast, cost-effective, and environmentally-friendly method. |
| 学科主题 | Chemistry ; Engineering |
| 收录类别 | SCI |
| 原文出处 | 10.1080/01496395.2015.1122634 |
| 公开日期 | 2016-05-06 |
| 源URL | [http://ir.xtbg.org.cn/handle/353005/9740]  |
| 专题 | 西双版纳热带植物园_文献共享 |
| 推荐引用方式 GB/T 7714 | Ye, Xiaolan,Cao, Di,Song, Fenyun,et al. Preparative separation of nine flavonoids from Pericarpium Citri Reticulatae by preparative-HPLC and HSCCC[J]. SEPARATION SCIENCE AND TECHNOLOGY,2016,51(5):807-815. |
| APA | Ye, Xiaolan,Cao, Di,Song, Fenyun,Fan, Guorong,&Wu, Fuhai.(2016).Preparative separation of nine flavonoids from Pericarpium Citri Reticulatae by preparative-HPLC and HSCCC.SEPARATION SCIENCE AND TECHNOLOGY,51(5),807-815. |
| MLA | Ye, Xiaolan,et al."Preparative separation of nine flavonoids from Pericarpium Citri Reticulatae by preparative-HPLC and HSCCC".SEPARATION SCIENCE AND TECHNOLOGY 51.5(2016):807-815. |
入库方式： OAI收割
来源：西双版纳热带植物园
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