A single-step isolation of squalene from olive oil deodorizer distillates by using centrifugal partition chromatography
文献类型:期刊论文
作者 | Xynos, Nikos ; Zervos, Michail ; Angelis, Apostolis ; Aligiannis, Nektarios ; Skaltsounis, Alexios-Leandros |
刊名 | SEPARATION SCIENCE AND TECHNOLOGY
![]() |
出版日期 | 2016 |
卷号 | 51期号:5页码:830-835 |
关键词 | COUNTER-CURRENT CHROMATOGRAPHY EXTRACTION COMPONENTS SEPARATION RECOVERY CARBON SEBUM |
ISSN号 | 0149-6395 |
中文摘要 | High added-value squalene (SQ) was purified in one step from olive oil deodorizer distillates (OODD) using preparative centrifugal partition chromatography (CPC) method, operating in the dual mode. The fractionation was performed using a non-aqueous biphasic solvent system consisting of heptane-acetonitrile-butanol (1.8:1.4:0.7, v/v/v), leading to the isolation of the target compound in 4 hours, using a preparative 1L column. Furthermore, a fast UHPLC-DAD method was developed and applied for the identification and quantification of SQ in both OODD and purified form. The content of SQ in the initial material was 23.4%, while the purity of the isolated SQ was 95.5%. The recovery of SQ was calculated at 76.3%. The productivity of the process was calculated at 234 mg/h/L. |
学科主题 | Chemistry ; Engineering |
收录类别 | SCI |
原文出处 | 10.1080/01496395.2015.1119843 |
公开日期 | 2016-05-06 |
源URL | [http://ir.xtbg.org.cn/handle/353005/9741] ![]() |
专题 | 西双版纳热带植物园_文献共享 |
推荐引用方式 GB/T 7714 | Xynos, Nikos,Zervos, Michail,Angelis, Apostolis,et al. A single-step isolation of squalene from olive oil deodorizer distillates by using centrifugal partition chromatography[J]. SEPARATION SCIENCE AND TECHNOLOGY,2016,51(5):830-835. |
APA | Xynos, Nikos,Zervos, Michail,Angelis, Apostolis,Aligiannis, Nektarios,&Skaltsounis, Alexios-Leandros.(2016).A single-step isolation of squalene from olive oil deodorizer distillates by using centrifugal partition chromatography.SEPARATION SCIENCE AND TECHNOLOGY,51(5),830-835. |
MLA | Xynos, Nikos,et al."A single-step isolation of squalene from olive oil deodorizer distillates by using centrifugal partition chromatography".SEPARATION SCIENCE AND TECHNOLOGY 51.5(2016):830-835. |
入库方式: OAI收割
来源:西双版纳热带植物园
浏览0
下载0
收藏0
其他版本
除非特别说明,本系统中所有内容都受版权保护,并保留所有权利。