Evaluation of a silicon oxynitride hydrophilic interaction liquid chromatography column in saccharide and glycoside separations
文献类型：期刊论文
| 作者 | Wan, Huihui1; Sheng, Qianying2; Zhong, Hongmin1; Guo, Xiujie3; Fu, Qing2; Liu, Yanfang3; Xue, Xingya3; Liang, Xinmiao3 |
| 刊名 | journal of separation science
 |
| 出版日期 | 2015-04-01 |
| 卷号 | 38期号:8页码:1271-1276 |
| 关键词 | Carbohydrates Hydrophilic interaction liquid chromatography Silica Silicon oxynitride Stationary phases |
| 英文摘要 | the retention characteristics of a silicon oxynitride stationary phase for carbohydrate separation were studied in hydrophilic interaction chromatography mode. four saccharides including mono-, di-, and trisaccharides were employed to investigate the effects of water content and buffer concentration in the mobile phase on hydrophilic interaction liquid chromatography retention. for the tested saccharides, the silicon oxynitride column demonstrated excellent performance in terms of separation efficiency, hydrophilicity, and interesting separation selectivity for carbohydrates compared to the bare silica stationary phase. finally, the silicon oxynitride hydrophilic interaction liquid chromatography column was employed in the separation of complex samples of fructooligosaccharides, saponins, and steviol glycoside from natural products. the resulting chromatograms demonstrated good separation efficiency and longer retention compared with silica, which further confirmed the advantages and potential application of silicon oxynitride stationary phase for hydrophilic interaction liquid chromatography separation. |
| WOS标题词 | science & technology ; physical sciences |
| 类目[WOS] | chemistry, analytical |
| 研究领域[WOS] | chemistry |
| 关键词[WOS] | anion-exchange chromatography ; stationary phases ; mass-spectrometry ; polar compounds ; performance ; selectivity ; retention ; surface ; metabolomics ; peptides |
| 收录类别 | SCI |
| 语种 | 英语 |
| WOS记录号 | WOS:000353488200002 |
| 公开日期 | 2016-05-09 |
| 源URL | [http://cas-ir.dicp.ac.cn/handle/321008/146189]  |
| 专题 | 大连化学物理研究所_中国科学院大连化学物理研究所 |
| 作者单位 | 1.Dalian Univ Technol, Analyt Ctr, Fac Chem Environm & Biol Sci & Technol, Dalian 116024, Peoples R China 2.E China Univ Sci & Technol, Engn Res Ctr Pharmaceut Proc Chem, Minist Educ, Sch Pharm, Shanghai 200237, Peoples R China 3.Chinese Acad Sci, Dalian Inst Chem Phys, Key Lab Separat Sci Analyt Chem, Dalian, Peoples R China |
| 推荐引用方式 GB/T 7714 | Wan, Huihui,Sheng, Qianying,Zhong, Hongmin,et al. Evaluation of a silicon oxynitride hydrophilic interaction liquid chromatography column in saccharide and glycoside separations[J]. journal of separation science,2015,38(8):1271-1276. |
| APA | Wan, Huihui.,Sheng, Qianying.,Zhong, Hongmin.,Guo, Xiujie.,Fu, Qing.,...&Liang, Xinmiao.(2015).Evaluation of a silicon oxynitride hydrophilic interaction liquid chromatography column in saccharide and glycoside separations.journal of separation science,38(8),1271-1276. |
| MLA | Wan, Huihui,et al."Evaluation of a silicon oxynitride hydrophilic interaction liquid chromatography column in saccharide and glycoside separations".journal of separation science 38.8(2015):1271-1276. |
入库方式： OAI收割
来源：大连化学物理研究所
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