Characterisation of oligosaccharides from Baizhu by HILIC-MS
文献类型：期刊论文
| 作者 | Lin, Zhe1; Liu, Yan-Fang2; Qu, Yang1; Shi, Li-Ying2; Dou, De-Qiang1; Kuang, Hai-Xue3 |
| 刊名 | natural product research
 |
| 出版日期 | 2015-07-03 |
| 卷号 | 29期号:13页码:1194-1200 |
| 关键词 | inulin-type oligosaccharides Atractylodes macrocephala Koidz XAmide column spleen lymphocyte transformation |
| 英文摘要 | polysaccharides from baizhu were separated by preparative hydrophilic interaction liquid chromatography on an xamide column and its components were characterised as inulin-type polysaccharides with structures of alpha-d-glucopyranosyl-[-(1 -> 2) -beta-d-fructofuranosyl-](n-1)-(1 -> 2) -beta-d-fructofuranoside (n=3-20) by a combinatory application of electrospray-ionisation mass spectrometry, nuclear magnetic resonance and ir, as well as the chemical analysis of monosaccharide composition. in addition, the contents of nystose and 1f-fructofranosylnystose in the crude and purified baizhu polysaccharides were determined to be 5.81%, 4.92% and 0.70%, 0.84% (w/w), respectively. in addition, mtt assay indicated that the baizhu polysaccharides could effectively promote spleen lymphocyte transformation for the enhancement of organism immunity. it is for the first time that inulin-type polysaccharides were discovered in baizhu and its immuno-enhancing activity was reported, which is a vigorous evidence to explain the efficacy of baizhu. |
| WOS标题词 | science & technology ; physical sciences ; life sciences & biomedicine |
| 类目[WOS] | chemistry, applied ; chemistry, medicinal |
| 研究领域[WOS] | chemistry ; pharmacology & pharmacy |
| 关键词[WOS] | fractions |
| 收录类别 | SCI |
| 语种 | 英语 |
| WOS记录号 | WOS:000356374300002 |
| 公开日期 | 2016-05-09 |
| 源URL | [http://cas-ir.dicp.ac.cn/handle/321008/146338]  |
| 专题 | 大连化学物理研究所_中国科学院大连化学物理研究所 |
| 作者单位 | 1.Liaoning Univ Tradit Chinese Med, Coll Pharm, Dalian 116600, Peoples R China 2.Chinese Acad Sci, Dalian Inst Chem Phys, Dalian 116023, Peoples R China 3.Heilongjiang Univ Chinese Med, Coll Pharm, Harbin 150000, Peoples R China |
| 推荐引用方式 GB/T 7714 | Lin, Zhe,Liu, Yan-Fang,Qu, Yang,et al. Characterisation of oligosaccharides from Baizhu by HILIC-MS[J]. natural product research,2015,29(13):1194-1200. |
| APA | Lin, Zhe,Liu, Yan-Fang,Qu, Yang,Shi, Li-Ying,Dou, De-Qiang,&Kuang, Hai-Xue.(2015).Characterisation of oligosaccharides from Baizhu by HILIC-MS.natural product research,29(13),1194-1200. |
| MLA | Lin, Zhe,et al."Characterisation of oligosaccharides from Baizhu by HILIC-MS".natural product research 29.13(2015):1194-1200. |
入库方式： OAI收割
来源：大连化学物理研究所
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