Simplified hydrothermal synthesis and optical properties of core-shell ZnS microspheres
文献类型：期刊论文
| 作者 | Li, Maohua1,2; Lu, Yi1,2; Hao JY(郝俊英)3 ; Long, Zerong2; Yang, Bo2; Liu, Yumei1; Hao JY(郝俊英)
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| 刊名 | OPTOELECTRONICS AND ADVANCED MATERIALS-RAPID COMMUNICATIONS
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| 出版日期 | 2014 |
| 卷号 | 8期号:11-12页码:1091-1095 |
| 关键词 | Hydrothermal Reaction Core-Shell Structure ZnS Glycerin |
| ISSN号 | 1842-6573 |
| 通讯作者 | 郝俊英 ; Liu, Yumei |
| 英文摘要 | Zinc acetylacetonate and thiourea are reacted in a 30:10 mixed water: glycerin solvent for 12 hours at 130 C to synthesize "core-shell" ZnS microspheres. The ZnS microspheres are characterized by scanning electron microscopy (SEM), transmission electron microscopy (TEM), x-ray diffraction (XRD), x-ray photoelectron spectroscopy (XPS), energy dispersive x-ray (EDX), high-resolution transmission electron microscopy (HRTEM); and selected area electron diffraction (SEAD). Ultraviolet-visible spectra (UV-vis) and photoluminescence spectroscopy (PL) were used in an optical study of the product. The results show that the synthesized ZnS microspheres have a diameter of 3-5 micrometers, a smooth shell surface, and an inner core structure. The existence of glycerin is crucial to the formation of spherical ZnS. no spherical particles are obtained in reaction systems without glycerin, and a decrease in glycerin content of the system reduces the yield of spherical products. |
| 收录类别 | SCI |
| 资助信息 | the National Natural Science Foundation of China (No. 51375471);the major project of Xinjiang Bureau of Quality and Technical Supervision (No. 2013-01);the Acience and Technology Project of State Quality Inspection Administration (2013QK086) |
| 语种 | 英语 |
| WOS记录号 | WOS:000347510200021 |
| 源URL | [http://210.77.64.217/handle/362003/20709]  |
| 专题 | 兰州化学物理研究所_固体润滑国家重点实验室 |
| 通讯作者 | Hao JY(郝俊英) |
| 作者单位 | 1.Xinjiang Univ, Coll Chem & Chem Engn, Urumqi Xinjing 830046, Peoples R China 2.Xinjiang Supervis & Inspect Inst Prod Qual, Urumqi Xinjing 830011, Peoples R China 3.Chinese Acad Sci, Lanzhou Inst Chem Phys, State key Lab Solid Lubricat, Lanzhou 730000, Peoples R China |
| 推荐引用方式 GB/T 7714 | Li, Maohua,Lu, Yi,Hao JY,et al. Simplified hydrothermal synthesis and optical properties of core-shell ZnS microspheres[J]. OPTOELECTRONICS AND ADVANCED MATERIALS-RAPID COMMUNICATIONS,2014,8(11-12):1091-1095. |
| APA | Li, Maohua.,Lu, Yi.,Hao JY.,Long, Zerong.,Yang, Bo.,...&郝俊英.(2014).Simplified hydrothermal synthesis and optical properties of core-shell ZnS microspheres.OPTOELECTRONICS AND ADVANCED MATERIALS-RAPID COMMUNICATIONS,8(11-12),1091-1095. |
| MLA | Li, Maohua,et al."Simplified hydrothermal synthesis and optical properties of core-shell ZnS microspheres".OPTOELECTRONICS AND ADVANCED MATERIALS-RAPID COMMUNICATIONS 8.11-12(2014):1091-1095. |
入库方式： OAI收割
来源：兰州化学物理研究所
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