Improved Stability of Emulsions in Preparation of Uniform Small-Sized Konjac Glucomanna (KGM) Microspheres with Epoxy-Based Polymer Membrane by Premix Membrane Emulsification
文献类型：期刊论文
| 作者 | Mi, Yace1,2; Li, Juan1; Zhou, Weiqing1; Zhang, Rongyue1; Ma, Guanghui1; Su, Zhiguo1 |
| 刊名 | POLYMERS
 |
| 出版日期 | 2016-03-01 |
| 卷号 | 8期号:3页码:1 |
| 关键词 | uniform small-sized KGM microspheres Epoxy-based polymer membrane (EP) alkaline condition premix membrane emulsification |
| ISSN号 | 2073-4360 |
| 英文摘要 | Uniform small-sized (<10 mu m) Konjac glucomanna (KGM) microspheres have great application prospects in bio-separation, drug delivery and controlled release. Premix membrane emulsification is an effective method to prepare uniform small-sized KGM microspheres. However, since KGM solution bears strong alkalinity, it requires the membrane to have a hydrophobic surface resistant to alkali. In this study, uniform small-sized KGM microspheres were prepared with epoxy-based polymer membrane (EP) we developed by premix membrane emulsification. It was found that emulsion coalescence and flocculation occurred frequently due to the high interface energy and sedimentation velocity of KGM emulsions. Emulsion stability had a significant influence on the uniformity and dispersity of the final KGM microspheres. To improve the stability of the emulsions, the effects of the concentration of the emulsifier, the viscosity of the KGM solution, the oil phase composition and the feeding method of epoxy chloropropane (EC) on the preparation results were studied. Under optimal preparation conditions (emulsifier 5 wt % PO-5s, KGM III (145.6 mPa center dot s), weight ratio of liquid paraffin (LP) to petroleum ether (PE) 11:1), uniform and stable KGM emulsions (d = 7.47 mu m, CV = 15.35%) were obtained and crosslinked without emulsion-instable phenomena. |
| WOS标题词 | Science & Technology ; Physical Sciences |
| 类目[WOS] | Polymer Science |
| 研究领域[WOS] | Polymer Science |
| 关键词[WOS] | ACID |
| 收录类别 | SCI |
| 语种 | 英语 |
| WOS记录号 | WOS:000373711700010 |
| 源URL | [http://ir.ipe.ac.cn/handle/122111/20997]  |
| 专题 | 过程工程研究所_生化工程国家重点实验室 |
| 作者单位 | 1.Chinese Acad Sci, Inst Proc Engn, Natl Key Lab Biochem Engn, Beijing 100190, Peoples R China 2.Univ Chinese Acad Sci, Beijing 100049, Peoples R China |
| 推荐引用方式 GB/T 7714 | Mi, Yace,Li, Juan,Zhou, Weiqing,et al. Improved Stability of Emulsions in Preparation of Uniform Small-Sized Konjac Glucomanna (KGM) Microspheres with Epoxy-Based Polymer Membrane by Premix Membrane Emulsification[J]. POLYMERS,2016,8(3):1. |
| APA | Mi, Yace,Li, Juan,Zhou, Weiqing,Zhang, Rongyue,Ma, Guanghui,&Su, Zhiguo.(2016).Improved Stability of Emulsions in Preparation of Uniform Small-Sized Konjac Glucomanna (KGM) Microspheres with Epoxy-Based Polymer Membrane by Premix Membrane Emulsification.POLYMERS,8(3),1. |
| MLA | Mi, Yace,et al."Improved Stability of Emulsions in Preparation of Uniform Small-Sized Konjac Glucomanna (KGM) Microspheres with Epoxy-Based Polymer Membrane by Premix Membrane Emulsification".POLYMERS 8.3(2016):1. |
入库方式： OAI收割
来源：过程工程研究所
浏览0
下载0
收藏0
其他版本
除非特别说明，本系统中所有内容都受版权保护，并保留所有权利。