Rapid analysis of biogenic amines from rice wine with isotope-coded derivatization followed by high performance liquid chromatography-tandem mass spectrometry
文献类型:期刊论文
作者 | Cai, Yiping1; Sun, Zhiwei1; Chen, Guang2; Liu, Xiaomei2; You, Jinmao2,3; Zhang, Caiqing4 |
刊名 | food chemistry
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出版日期 | 2016-02-01 |
卷号 | 192页码:388-394 |
关键词 | Biogenic amines (BAs) High-performance liquid chromatography-tandem mass spectrometry (HPLC-MS/MS) Isotope-coded derivatization reagent Chinese rice wine |
英文摘要 | a pair of isotope-coded derivatization reagents, d(0)-10-methyl-acridone-2-sulfonyl chloride (d(0)-masc, light form) and d(3)-10-methyl-acridone-2-sulfonyl chloride (d(3)-masc, heavy form), were used for labeling biogenic amines (bas). on basis of the isotope-coded derivatization, a global isotope internal standard quantitative method for determining seven bas by high-performance liquid chromatography-tandem mass spectrometry (hplc-ms/ms) was developed. the d(0)-masc and d(3)-masc can easily label bas under mild conditions within 15 min at 50 degrees c. the obtained light and heavy labeled bas were monitored by the transitions of [m+h](+) -> 208 and [m+h](+) -> 211, respectively. relative quantification of bas was achieved by calculation of the peak area ratios of d(0)-masc/d(3)-masc labeled derivatives. excellent linear responses for relative quantification were observed in the range of 1/10-10/1. the developed method has been successfully applied to the quantification of bas in chinese rice wine with recoveries ranging from 94.9% to 104.5%. (c) 2015 elsevier ltd. all rights reserved. |
WOS标题词 | science & technology ; physical sciences ; life sciences & biomedicine |
类目[WOS] | chemistry, applied ; food science & technology ; nutrition & dietetics |
研究领域[WOS] | chemistry ; food science & technology ; nutrition & dietetics |
关键词[WOS] | fluorescence detection ; foods ; samples ; cheese |
收录类别 | SCI |
语种 | 英语 |
WOS记录号 | WOS:000362304500052 |
源URL | [http://ir.nwipb.ac.cn/handle/363003/6528] ![]() |
专题 | 西北高原生物研究所_中国科学院西北高原生物研究所 |
作者单位 | 1.Qufu Normal Univ, Key Lab Life Organ Anal Shandong Prov, Qufu 273165, Peoples R China 2.Key Lab Pharmaceut Intermediates & Nat Prod, Qufu 273165, Peoples R China 3.Chinese Acad Sci, Northwest Inst Plateau Biol, Xining, Peoples R China 4.Shandong Univ, Qianfoshan Hosp, Jinan 250100, Peoples R China |
推荐引用方式 GB/T 7714 | Cai, Yiping,Sun, Zhiwei,Chen, Guang,et al. Rapid analysis of biogenic amines from rice wine with isotope-coded derivatization followed by high performance liquid chromatography-tandem mass spectrometry[J]. food chemistry,2016,192:388-394. |
APA | Cai, Yiping,Sun, Zhiwei,Chen, Guang,Liu, Xiaomei,You, Jinmao,&Zhang, Caiqing.(2016).Rapid analysis of biogenic amines from rice wine with isotope-coded derivatization followed by high performance liquid chromatography-tandem mass spectrometry.food chemistry,192,388-394. |
MLA | Cai, Yiping,et al."Rapid analysis of biogenic amines from rice wine with isotope-coded derivatization followed by high performance liquid chromatography-tandem mass spectrometry".food chemistry 192(2016):388-394. |
入库方式: OAI收割
来源:西北高原生物研究所
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