中国科学院机构知识库网格
Chinese Academy of Sciences Institutional Repositories Grid
Rapid analysis of biogenic amines from rice wine with isotope-coded derivatization followed by high performance liquid chromatography-tandem mass spectrometry

文献类型:期刊论文

作者Cai, Yiping1; Sun, Zhiwei1; Chen, Guang2; Liu, Xiaomei2; You, Jinmao2,3; Zhang, Caiqing4
刊名food chemistry
出版日期2016-02-01
卷号192页码:388-394
关键词Biogenic amines (BAs) High-performance liquid chromatography-tandem mass spectrometry (HPLC-MS/MS) Isotope-coded derivatization reagent Chinese rice wine
英文摘要a pair of isotope-coded derivatization reagents, d(0)-10-methyl-acridone-2-sulfonyl chloride (d(0)-masc, light form) and d(3)-10-methyl-acridone-2-sulfonyl chloride (d(3)-masc, heavy form), were used for labeling biogenic amines (bas). on basis of the isotope-coded derivatization, a global isotope internal standard quantitative method for determining seven bas by high-performance liquid chromatography-tandem mass spectrometry (hplc-ms/ms) was developed. the d(0)-masc and d(3)-masc can easily label bas under mild conditions within 15 min at 50 degrees c. the obtained light and heavy labeled bas were monitored by the transitions of [m+h](+) -> 208 and [m+h](+) -> 211, respectively. relative quantification of bas was achieved by calculation of the peak area ratios of d(0)-masc/d(3)-masc labeled derivatives. excellent linear responses for relative quantification were observed in the range of 1/10-10/1. the developed method has been successfully applied to the quantification of bas in chinese rice wine with recoveries ranging from 94.9% to 104.5%. (c) 2015 elsevier ltd. all rights reserved.
WOS标题词science & technology ; physical sciences ; life sciences & biomedicine
类目[WOS]chemistry, applied ; food science & technology ; nutrition & dietetics
研究领域[WOS]chemistry ; food science & technology ; nutrition & dietetics
关键词[WOS]fluorescence detection ; foods ; samples ; cheese
收录类别SCI
语种英语
WOS记录号WOS:000362304500052
源URL[http://ir.nwipb.ac.cn/handle/363003/6528]  
专题西北高原生物研究所_中国科学院西北高原生物研究所
作者单位1.Qufu Normal Univ, Key Lab Life Organ Anal Shandong Prov, Qufu 273165, Peoples R China
2.Key Lab Pharmaceut Intermediates & Nat Prod, Qufu 273165, Peoples R China
3.Chinese Acad Sci, Northwest Inst Plateau Biol, Xining, Peoples R China
4.Shandong Univ, Qianfoshan Hosp, Jinan 250100, Peoples R China
推荐引用方式
GB/T 7714
Cai, Yiping,Sun, Zhiwei,Chen, Guang,et al. Rapid analysis of biogenic amines from rice wine with isotope-coded derivatization followed by high performance liquid chromatography-tandem mass spectrometry[J]. food chemistry,2016,192:388-394.
APA Cai, Yiping,Sun, Zhiwei,Chen, Guang,Liu, Xiaomei,You, Jinmao,&Zhang, Caiqing.(2016).Rapid analysis of biogenic amines from rice wine with isotope-coded derivatization followed by high performance liquid chromatography-tandem mass spectrometry.food chemistry,192,388-394.
MLA Cai, Yiping,et al."Rapid analysis of biogenic amines from rice wine with isotope-coded derivatization followed by high performance liquid chromatography-tandem mass spectrometry".food chemistry 192(2016):388-394.

入库方式: OAI收割

来源:西北高原生物研究所

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