Quick method for separating target compounds from the bark of Maqian (Zanthoxylum myriacanthum var. pubescens) by high-performance countercurrent chromatography
文献类型：期刊论文
| 作者 | Huabin Hu ; Qishi Song; Youkai Xu
|
| 刊名 | JOURNAL OF SEPARATION SCIENCE
 |
| 出版日期 | 2016 |
| 卷号 | 39期号:20页码:4049-4052 |
| 中文摘要 | Choosing a suitable solvent system for a countercurrent chromatography separation presents a challenge for many researchers. In this study, we introduce a quick method of separating a target compound from the bark of Zanthoxylum myriacanthum var. pubescens by countercurrent chromatography. This method relies on the thin-layer chromatography based generally useful estimation of solvent systems. This paper will present how to quickly choose a suitable solvent system with a thin-layer chromatography based generally useful estimation of solvent systems working chart. O-Methyltembamide (1) was enriched by countercurrent chromatography using n-hexane/ethyl acetate/methanol/water (6:4:6:4) as the solvent system. Further purification was achieved by high-performance liquid chromatography with purities of 98.2% from Z. myriacanthum var. pubescens bark. |
| 公开日期 | 2016-11-30 |
| 源URL | [http://ir.xtbg.org.cn/handle/353005/10102]  |
| 专题 | 西双版纳热带植物园_民族植物学研究组 中国科学院西双版纳热带植物园 |
| 推荐引用方式 GB/T 7714 | Huabin Hu,Qishi Song,Youkai Xu. Quick method for separating target compounds from the bark of Maqian (Zanthoxylum myriacanthum var. pubescens) by high-performance countercurrent chromatography[J]. JOURNAL OF SEPARATION SCIENCE,2016,39(20):4049-4052. |
| APA | Huabin Hu,Qishi Song,&Youkai Xu.(2016).Quick method for separating target compounds from the bark of Maqian (Zanthoxylum myriacanthum var. pubescens) by high-performance countercurrent chromatography.JOURNAL OF SEPARATION SCIENCE,39(20),4049-4052. |
| MLA | Huabin Hu,et al."Quick method for separating target compounds from the bark of Maqian (Zanthoxylum myriacanthum var. pubescens) by high-performance countercurrent chromatography".JOURNAL OF SEPARATION SCIENCE 39.20(2016):4049-4052. |
入库方式： OAI收割
来源：西双版纳热带植物园
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