Preparation of SiOC/HfO2 fibers from silicon alkoxides and tetrachloride hafnium by a sol-gel process
文献类型:期刊论文
作者 | Xiao Yan; Dong Su; Haozhi Duan; Fengrui Zhang |
刊名 | Materials Letters
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出版日期 | 2015 |
英文摘要 | This study presents fabrication and characterization of novel SiOC/HfO2 fibers by a sal-gel process. Polyhafnosiloxane (PHfSO) fibers have been drawn from silicon alkoxide solution consisting oftetraethoxylsilane (TEOS) and dimethyldiethoxylsilane (DMDES) using tetrachloride hafnium (HfCl4) ashafnium source. The spinnability of the solution has been optimized by varying the amount of HfCl4 and H2O. The Hf incorporation is confirmed by the formation of bridge through co-condensation of HfCl4, TEOS and DEDES. Subsequent pyrolysis treatment of the PHfSO gel fibers yields dense SiOC/HfO2 fibers with high ceramic yield of 81 wt%. The SiOC/HfO2 fibers exhibit good thermal stability up to 1500 degrees C and mechanical property with tensile strength of 930 MPa. |
收录类别 | SCI |
原文出处 | http://dx.doi.org/10.1016/j.matlet.2015.02.067 |
语种 | 英语 |
源URL | [http://ir.siat.ac.cn:8080/handle/172644/7561] ![]() |
专题 | 深圳先进技术研究院_南沙所 |
作者单位 | Materials Letters |
推荐引用方式 GB/T 7714 | Xiao Yan,Dong Su,Haozhi Duan,et al. Preparation of SiOC/HfO2 fibers from silicon alkoxides and tetrachloride hafnium by a sol-gel process[J]. Materials Letters,2015. |
APA | Xiao Yan,Dong Su,Haozhi Duan,&Fengrui Zhang.(2015).Preparation of SiOC/HfO2 fibers from silicon alkoxides and tetrachloride hafnium by a sol-gel process.Materials Letters. |
MLA | Xiao Yan,et al."Preparation of SiOC/HfO2 fibers from silicon alkoxides and tetrachloride hafnium by a sol-gel process".Materials Letters (2015). |
入库方式: OAI收割
来源:深圳先进技术研究院
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