中国科学院机构知识库网格
Chinese Academy of Sciences Institutional Repositories Grid
Effects of Sintering Atmosphere on the PLMNT Transparent Ceramics Prepared by Hot-Press Sintering Method

文献类型:期刊论文

作者Ji, Wenlong1; He, Xiyun1; Zeng, Xia1; Sun, Dazhi2; Cheng, Wenxiu1; Qiu, Pingsun1; Xia, Bin1; Sun, Xiaolong1; Wang, Dong1
刊名FERROELECTRICS
出版日期2016-01-02
卷号490期号:1页码:196-202
关键词PLMNT transparent ceramics hot-press sintering atmosphere sintering
英文摘要

La modified Pb(Mg1/3Nb2/3)O-3-PbTiO3 (PLMNT) transparent electro-optic (EO) ceramics with pure perovskite phase were fabricated by the uniaxial hot-press sintering method. An improved hot-press sintering technique with varied atmosphere was proposed to eliminate the pore defects. It consists of four stages: 1) sintering at a relatively low temperature (800 degrees C) in the vacuum atmosphere first, and then in the pure O-2 atmosphere; 2) sintering in a pure O-2 atmosphere at high temperature by uniaxial hot-press method; 3) replacing the O-2 atmosphere with CO2 gas to eliminate the residual closed pores; 4) finally exchanging CO2 atmosphere with pure O-2 gas to eliminate the oxygen vacancies. The research results certified that the thermal treatment in the vacuum atmosphere and CO2 atmosphere could eliminate the residual closed pores and improve the transmittance of the PLMNT transparent ceramics effectively. By the improved hot-press sintering technique, the optical transmittance of the polished PLMNT transparent ceramics with a thickness of 0.35mm increases from 61% to 64% at 632.8nm. The reasonable explanation was given about the mechanism of the improvements of this sintering technique.

WOS标题词Science & Technology ; Technology ; Physical Sciences
类目[WOS]Materials Science, Multidisciplinary ; Physics, Condensed Matter
研究领域[WOS]Materials Science ; Physics
关键词[WOS]FERROELECTRIC CERAMICS ; PLZT CERAMICS ; ELECTROOPTIC PROPERTIES ; FABRICATION ; IMPROVEMENTS
收录类别SCI
语种英语
WOS记录号WOS:000369189600022
源URL[http://ir.sic.ac.cn/handle/331005/23254]  
专题上海硅酸盐研究所_无机功能材料与器件重点实验室_期刊论文
作者单位1.Chinese Acad Sci, Shanghai Inst Ceram, Key Lab Inorgan Funct Mat & Devices, Shanghai 200050, Peoples R China
2.Shanghai Normal Univ, Dept Chem, Key Lab Resource Chem, Educ Minist, 100 Guilin Rd, Shanghai 200234, Peoples R China
推荐引用方式
GB/T 7714
Ji, Wenlong,He, Xiyun,Zeng, Xia,et al. Effects of Sintering Atmosphere on the PLMNT Transparent Ceramics Prepared by Hot-Press Sintering Method[J]. FERROELECTRICS,2016,490(1):196-202.
APA Ji, Wenlong.,He, Xiyun.,Zeng, Xia.,Sun, Dazhi.,Cheng, Wenxiu.,...&Wang, Dong.(2016).Effects of Sintering Atmosphere on the PLMNT Transparent Ceramics Prepared by Hot-Press Sintering Method.FERROELECTRICS,490(1),196-202.
MLA Ji, Wenlong,et al."Effects of Sintering Atmosphere on the PLMNT Transparent Ceramics Prepared by Hot-Press Sintering Method".FERROELECTRICS 490.1(2016):196-202.

入库方式: OAI收割

来源:上海硅酸盐研究所

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