Effects of Sintering Atmosphere on the PLMNT Transparent Ceramics Prepared by Hot-Press Sintering Method
文献类型:期刊论文
作者 | Ji, Wenlong1; He, Xiyun1; Zeng, Xia1; Sun, Dazhi2; Cheng, Wenxiu1; Qiu, Pingsun1; Xia, Bin1; Sun, Xiaolong1; Wang, Dong1 |
刊名 | FERROELECTRICS
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出版日期 | 2016-01-02 |
卷号 | 490期号:1页码:196-202 |
关键词 | PLMNT transparent ceramics hot-press sintering atmosphere sintering |
英文摘要 | La modified Pb(Mg1/3Nb2/3)O-3-PbTiO3 (PLMNT) transparent electro-optic (EO) ceramics with pure perovskite phase were fabricated by the uniaxial hot-press sintering method. An improved hot-press sintering technique with varied atmosphere was proposed to eliminate the pore defects. It consists of four stages: 1) sintering at a relatively low temperature (800 degrees C) in the vacuum atmosphere first, and then in the pure O-2 atmosphere; 2) sintering in a pure O-2 atmosphere at high temperature by uniaxial hot-press method; 3) replacing the O-2 atmosphere with CO2 gas to eliminate the residual closed pores; 4) finally exchanging CO2 atmosphere with pure O-2 gas to eliminate the oxygen vacancies. The research results certified that the thermal treatment in the vacuum atmosphere and CO2 atmosphere could eliminate the residual closed pores and improve the transmittance of the PLMNT transparent ceramics effectively. By the improved hot-press sintering technique, the optical transmittance of the polished PLMNT transparent ceramics with a thickness of 0.35mm increases from 61% to 64% at 632.8nm. The reasonable explanation was given about the mechanism of the improvements of this sintering technique. |
WOS标题词 | Science & Technology ; Technology ; Physical Sciences |
类目[WOS] | Materials Science, Multidisciplinary ; Physics, Condensed Matter |
研究领域[WOS] | Materials Science ; Physics |
关键词[WOS] | FERROELECTRIC CERAMICS ; PLZT CERAMICS ; ELECTROOPTIC PROPERTIES ; FABRICATION ; IMPROVEMENTS |
收录类别 | SCI |
语种 | 英语 |
WOS记录号 | WOS:000369189600022 |
源URL | [http://ir.sic.ac.cn/handle/331005/23254] ![]() |
专题 | 上海硅酸盐研究所_无机功能材料与器件重点实验室_期刊论文 |
作者单位 | 1.Chinese Acad Sci, Shanghai Inst Ceram, Key Lab Inorgan Funct Mat & Devices, Shanghai 200050, Peoples R China 2.Shanghai Normal Univ, Dept Chem, Key Lab Resource Chem, Educ Minist, 100 Guilin Rd, Shanghai 200234, Peoples R China |
推荐引用方式 GB/T 7714 | Ji, Wenlong,He, Xiyun,Zeng, Xia,et al. Effects of Sintering Atmosphere on the PLMNT Transparent Ceramics Prepared by Hot-Press Sintering Method[J]. FERROELECTRICS,2016,490(1):196-202. |
APA | Ji, Wenlong.,He, Xiyun.,Zeng, Xia.,Sun, Dazhi.,Cheng, Wenxiu.,...&Wang, Dong.(2016).Effects of Sintering Atmosphere on the PLMNT Transparent Ceramics Prepared by Hot-Press Sintering Method.FERROELECTRICS,490(1),196-202. |
MLA | Ji, Wenlong,et al."Effects of Sintering Atmosphere on the PLMNT Transparent Ceramics Prepared by Hot-Press Sintering Method".FERROELECTRICS 490.1(2016):196-202. |
入库方式: OAI收割
来源:上海硅酸盐研究所
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