Preparation and characterization of long methacrylate monolithic column for capillary liquid chromatography
文献类型：期刊论文
| 作者 | Shu, X; Chen, LX; Yang, BC; Guan, YF |
| 刊名 | journal of chromatography a
 |
| 出版日期 | 2004-10-15 |
| 卷号 | 1052期号:1-2页码:205-209 |
| 关键词 | monolithic column butyl methacrylate phase stationary phases LC |
| 产权排序 | 1;1 |
| 英文摘要 | long methacrylate monolithic columns (100 cm x 320 mum i.d.) were prepared from silanized fused-silica capillaries of 320 mum i.d. by in situ copolymerization of butyl methacrylate (bma) with ethylene dimethacrylate (edma) in the presence of a suitable porogen. the separation performance and selectivity of the column were evaluated and compared with a 25 cm x 320 mum i.d. column prepared in the same way by capillary high-performance liquid chromatography (mu-hplc) the results showed that the 1 m long monolithic column can generate 33 x 10(3) plate number and exhibited good permeability, higher sample loadability, and separation capability. (c) 2004 elsevier b.v. all rights reserved. |
| WOS标题词 | science & technology ; life sciences & biomedicine ; physical sciences |
| 类目[WOS] | biochemical research methods ; chemistry, analytical |
| 研究领域[WOS] | biochemistry & molecular biology ; chemistry |
| 关键词[WOS] | rod columns ; electrochromatography |
| 收录类别 | SCI |
| 原文出处 | true |
| 语种 | 英语 |
| WOS记录号 | WOS:000224501000025 |
| 公开日期 | 2010-11-30 |
| 源URL | [http://159.226.238.44/handle/321008/81703]  |
| 专题 | 大连化学物理研究所_中国科学院大连化学物理研究所 |
| 作者单位 | Chinese Acad Sci, Dalian Inst Chem Phys, Dept Analyt Chem & Micro Instrumentat, Dalian 116012, Peoples R China |
| 推荐引用方式 GB/T 7714 | Shu, X,Chen, LX,Yang, BC,et al. Preparation and characterization of long methacrylate monolithic column for capillary liquid chromatography[J]. journal of chromatography a,2004,1052(1-2):205-209. |
| APA | Shu, X,Chen, LX,Yang, BC,&Guan, YF.(2004).Preparation and characterization of long methacrylate monolithic column for capillary liquid chromatography.journal of chromatography a,1052(1-2),205-209. |
| MLA | Shu, X,et al."Preparation and characterization of long methacrylate monolithic column for capillary liquid chromatography".journal of chromatography a 1052.1-2(2004):205-209. |
入库方式： OAI收割
来源：大连化学物理研究所
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