Microwave-assisted hydrothermal synthesis of hydroxy-sodalite zeolite membrane
文献类型:期刊论文
作者 | Xu, XC; Bao, Y; Song, CS; Yang, WS; Liu, J; Lin, LW |
刊名 | microporous and mesoporous materials
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出版日期 | 2004-11-02 |
卷号 | 75期号:3页码:173-181 |
关键词 | gas separation hydrothermal synthesis hydroxy-sodalite microwave heating zeolite membrane |
产权排序 | 1;1 |
英文摘要 | a high quality pure hydroxy-sodalite zeolite membrane was successfully synthesized on an alpha-al2o3 support by a novel microwave-assisted hydrothermal synthesis (mars) method. influence of synthesis conditions, such as synthesis time, synthesis procedure, etc., on the formation of hydroxy-sodalite zeolite membrane by mahs method was studied by x-ray diffraction (xrd), scanning electron microscopy (sem) and gas permeation measurements. the synthesis of hydroxy-sodalite zeolite membrane by mahs method only needed 45 min and synthesis was more than 8 times faster than by the conventional hydrothermal synthesis (chs) method. a pure hydroxy-sodalite zeolite membrane was easily synthesized by mahs method, while a zeolite membrane, which consisted of nax zeolite, naa zeolite and hydroxy-sodalite zeolite, was usually synthesized by chs method. the effect of preparation procedures had a dramatic impact on the formation of hydroxy-sodalite zeolite membrane and a single-stage synthesis procedure produced a pure hydroxy-sodalite zeolite membrane. the pure hydroxy-sodalite zeolite membrane synthesized by mars method was found to be well inter-grown and the thickness of the membrane was 6-7 mum. gas permeation results showed that the hydrogen/n-butane permselectivity of the hydroxy-sodalite zeolite membrane was larger than 1000. (c) 2004 elsevier inc. all rights reserved. |
WOS标题词 | science & technology ; physical sciences ; technology |
类目[WOS] | chemistry, applied ; chemistry, physical ; nanoscience & nanotechnology ; materials science, multidisciplinary |
研究领域[WOS] | chemistry ; science & technology - other topics ; materials science |
关键词[WOS] | molecular-sieve membranes ; gas permeation properties ; inorganic membranes ; composite membranes ; mfi membranes ; separation ; alpo4-5 ; performance ; irradiation ; crystals |
收录类别 | SCI |
原文出处 | true |
语种 | 英语 |
WOS记录号 | WOS:000224824900001 |
公开日期 | 2010-11-30 |
源URL | [http://159.226.238.44/handle/321008/81785] ![]() |
专题 | 大连化学物理研究所_中国科学院大连化学物理研究所 |
作者单位 | 1.Penn State Univ, Energy Inst, Clean Fuels & Catalysis Program, University Pk, PA 16802 USA 2.Chinese Acad Sci, Dalian Inst Chem Phys, State Key Lab Catalysis, Dalian 116023, Peoples R China |
推荐引用方式 GB/T 7714 | Xu, XC,Bao, Y,Song, CS,et al. Microwave-assisted hydrothermal synthesis of hydroxy-sodalite zeolite membrane[J]. microporous and mesoporous materials,2004,75(3):173-181. |
APA | Xu, XC,Bao, Y,Song, CS,Yang, WS,Liu, J,&Lin, LW.(2004).Microwave-assisted hydrothermal synthesis of hydroxy-sodalite zeolite membrane.microporous and mesoporous materials,75(3),173-181. |
MLA | Xu, XC,et al."Microwave-assisted hydrothermal synthesis of hydroxy-sodalite zeolite membrane".microporous and mesoporous materials 75.3(2004):173-181. |
入库方式: OAI收割
来源:大连化学物理研究所
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