热门
Determination of 1-phenyl-3-methyl-5-pyrazolone-labeled carbohydrates by liquid chromatography and micellar electrokinetic chromatography
文献类型：期刊论文
| 作者 | Zhang, LY; Xu, J; Zhang, LH; Zhang, WB; Zhang, YK |
| 刊名 | journal of chromatography b-analytical technologies in the biomedical and life sciences
 |
| 出版日期 | 2003-08-05 |
| 卷号 | 793期号:1页码:159-165 |
| 关键词 | 1-phenyl-3-methyl-5-pyrazolone carbohydrates |
| 产权排序 | 1;1 |
| 英文摘要 | in this paper, the method for the derivatization of carbohydrates with 1-phenyl-3-methyl-5-pyrazolone (pmp) was simplified. one-third of the derivatization time was saved. five monosaccharide derivatives have been well separated by mekc and hplc under optimized conditions. good reproducibility could be obtained with relative standard deviation (rsd) values of the migration times within 5.0 and 2.3%, respectively. furthermore, the developed methods have been successfully applied to the analysis of carbohydrates in aloe powder and food. these methods are quite useful for routine analysis of monosaccharides and oligosaccharides in real samples. (c) 2003 elsevier b.v. all rights reserved. |
| WOS标题词 | science & technology ; life sciences & biomedicine ; physical sciences |
| 类目[WOS] | biochemical research methods ; chemistry, analytical |
| 研究领域[WOS] | biochemistry & molecular biology ; chemistry |
| 关键词[WOS] | capillary-electrophoresis ; derivatives ; derivatization ; sugars ; separation ; aldoses ; glycans ; acid ; hplc |
| 收录类别 | SCI |
| 原文出处 | true |
| 语种 | 英语 |
| WOS记录号 | WOS:000184525800014 |
| 公开日期 | 2010-11-30 |
| 源URL | [http://159.226.238.44/handle/321008/83489]  |
| 专题 | 大连化学物理研究所_中国科学院大连化学物理研究所 |
| 作者单位 | 1.Chinese Acad Sci, Dalian Inst Chem Phys, Natl Chromatog Res & Anal Ctr, Dalian 1116011, Peoples R China 2.Nanjing Univ Sci & Technol, Nanjing 210094, Peoples R China |
| 推荐引用方式 GB/T 7714 | Zhang, LY,Xu, J,Zhang, LH,et al. Determination of 1-phenyl-3-methyl-5-pyrazolone-labeled carbohydrates by liquid chromatography and micellar electrokinetic chromatography[J]. journal of chromatography b-analytical technologies in the biomedical and life sciences,2003,793(1):159-165. |
| APA | Zhang, LY,Xu, J,Zhang, LH,Zhang, WB,&Zhang, YK.(2003).Determination of 1-phenyl-3-methyl-5-pyrazolone-labeled carbohydrates by liquid chromatography and micellar electrokinetic chromatography.journal of chromatography b-analytical technologies in the biomedical and life sciences,793(1),159-165. |
| MLA | Zhang, LY,et al."Determination of 1-phenyl-3-methyl-5-pyrazolone-labeled carbohydrates by liquid chromatography and micellar electrokinetic chromatography".journal of chromatography b-analytical technologies in the biomedical and life sciences 793.1(2003):159-165. |
入库方式： OAI收割
来源：大连化学物理研究所
浏览0
下载0
收藏0
其他版本
除非特别说明，本系统中所有内容都受版权保护，并保留所有权利。