Analysis of five glycosides in Swertin franchetiana H. Smith extracts by high performance liquid chromatography and atmospheric pressure chemical ionization-mass spectrometry
文献类型:期刊论文
作者 | Wei, T; Dahua, Z; Cheng, XG; Li, YL; Chen, LR; Li, YM |
刊名 | chinese journal of analytical chemistry
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出版日期 | 2005-09-01 |
卷号 | 33期号:9页码:1265-1268 |
关键词 | liquid chromatography-mass spectrometry glycosides extract of swertia franchetiana H. Smith |
英文摘要 | a rapid method was first applied to analyze the extract of the swertia franchetiana h. smith with high performance liquid chromatograghy-atmospheric pressure(lc-apci-ms) and ultraviolet (uv) spectrometry. five glycosides were well separated on an ods column (4. 6 mm i.d. x 200 mm, 5 mu m) with mixtures of methanol and water as mobile phase. the recoveries of (1) swertiamarin (2) gentiopicroside (3) sweroside (4) isoorientin and (5) swetianolin fortified in the ranges of 7. 4 similar to 740; 14 similar to 590; 5.2 similar to 525; 4.2 similar to 343; and 1.0 similar to 171 mg/l were 98.3%, 106.7%, 92.3%, 88.2% and 107.3%, respectively. it is suitable for the quality control of the extract from swertia franchetiana h. smith. |
WOS标题词 | science & technology ; physical sciences |
类目[WOS] | chemistry, analytical |
研究领域[WOS] | chemistry |
收录类别 | SCI |
语种 | 英语 |
WOS记录号 | WOS:000232564600015 |
源URL | [http://ir.nwipb.ac.cn/handle/363003/6849] ![]() |
专题 | 西北高原生物研究所_中国科学院西北高原生物研究所 |
作者单位 | 1.Chinese Acad Sci, Lanzhou Inst Chem Phys, Lanzhou 730000, Peoples R China 2.Gansu Inst Drug Control, Lanzhou 730030, Peoples R China 3.PetroChina Co Ltd Lubricant Co, Lanzhou 730060, Peoples R China 4.Chinese Acad Sci, NW Plateau Inst Biol, Xining 810001, Peoples R China |
推荐引用方式 GB/T 7714 | Wei, T,Dahua, Z,Cheng, XG,et al. Analysis of five glycosides in Swertin franchetiana H. Smith extracts by high performance liquid chromatography and atmospheric pressure chemical ionization-mass spectrometry[J]. chinese journal of analytical chemistry,2005,33(9):1265-1268. |
APA | Wei, T,Dahua, Z,Cheng, XG,Li, YL,Chen, LR,&Li, YM.(2005).Analysis of five glycosides in Swertin franchetiana H. Smith extracts by high performance liquid chromatography and atmospheric pressure chemical ionization-mass spectrometry.chinese journal of analytical chemistry,33(9),1265-1268. |
MLA | Wei, T,et al."Analysis of five glycosides in Swertin franchetiana H. Smith extracts by high performance liquid chromatography and atmospheric pressure chemical ionization-mass spectrometry".chinese journal of analytical chemistry 33.9(2005):1265-1268. |
入库方式: OAI收割
来源:西北高原生物研究所
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