Characterization of saccharides and phenolic acids in the Chinese herb Tanshen by ESI-FT-ICR-MS and HPLC
文献类型：期刊论文
| 作者 | Li HL ; Song FR ; Zheng Z ; Liu ZQ ; Liu SY |
| 刊名 | journal of mass spectrometry
 |
| 出版日期 | 2008 |
| 卷号 | 43期号:11页码:1545-1552 |
| ISSN号 | 1076-5174 |
| 关键词 | ELECTROSPRAY MASS-SPECTROMETRY RADIX-SALVIAE-MILTIORRHIZAE N-LINKED GLYCANS NEGATIVE-IONS IDENTIFICATION FRAGMENTATION RATS OLIGOSACCHARIDES CONSTITUENTS ADDUCTS |
| 通讯作者 | liu hl |
| 中文摘要 | this study sought to determine the main components (saccharides and phenolic acids) in crude extract of the chinese herb tanshen by electrospray ionization fourier transform ion cyclotron resonant mass spectrometry (esi-ft-icr-ms) in negative-ion mode. eleven compounds were identified as phenolic acids by exact mass measurement and further confirmed by sustained off-resonance irradiation (sori) cid data. in addition, monosaccharicles and oligosaccharides (n = 2 similar to 5) and a serial of corresponding anionic adducts of saccharide were observed without adding any anions additionally to the extract solution, and the anionic components were unambiguously identified as h2o, hcl, hcooh, hno3, c3h6o2, h2so4 and c5h7no3 according to the exact mass measurement results. |
| 收录类别 | SCI |
| 语种 | 英语 |
| WOS记录号 | WOS:000261070400010 |
| 公开日期 | 2010-04-14 |
| 源URL | [http://ir.ciac.jl.cn/handle/322003/10609]  |
| 专题 | 长春应用化学研究所_长春应用化学研究所知识产出_期刊论文 |
| 推荐引用方式 GB/T 7714 | Li HL,Song FR,Zheng Z,et al. Characterization of saccharides and phenolic acids in the Chinese herb Tanshen by ESI-FT-ICR-MS and HPLC[J]. journal of mass spectrometry,2008,43(11):1545-1552. |
| APA | Li HL,Song FR,Zheng Z,Liu ZQ,&Liu SY.(2008).Characterization of saccharides and phenolic acids in the Chinese herb Tanshen by ESI-FT-ICR-MS and HPLC.journal of mass spectrometry,43(11),1545-1552. |
| MLA | Li HL,et al."Characterization of saccharides and phenolic acids in the Chinese herb Tanshen by ESI-FT-ICR-MS and HPLC".journal of mass spectrometry 43.11(2008):1545-1552. |
入库方式： OAI收割
来源：长春应用化学研究所
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