Studies on the stability of diester-diterpenoid alkaloids from the genus Aconitum L. by high performance liquid chromatography combined with electrospray ionisation tandem mass spectrometry (HPLC/ESI/MSn)
文献类型：期刊论文
| 作者 | Yue H ; Pi ZF ; Li HL ; Song FR ; Liu ZQ ; Liu SY |
| 刊名 | phytochemical analysis
 |
| 出版日期 | 2008 |
| 卷号 | 19期号:2页码:141-147 |
| 关键词 | CHINESE MEDICINES MESACONITINE SEPARATION EXTRACT URINE SERUM |
| ISSN号 | 0958-0344 |
| 通讯作者 | liu sy |
| 中文摘要 | the stability of diester-diterpenoid alkaloids (dda) from plants of the genus aconitum l. has been studied in different solvents and ph buffers. the hplc/esims method for analysing the concentration of dda was established and dda's decomposition products were elucidated by hplc/esi-ms/msn. in different solvents, e.g. dichloromethane, ether, methanol and distilled water, the decomposition pathways of dda are quite different and their difference in stabilities depends on the difference of their structures, in which substituents at the n atom and substituents at c-3 are different. the pyrolytic products of dda, such as deacetoxy aconitine-type alkaloids, have been observed in the above solvents, whereas 8-methoxy-14-benzoyl aconitine-type alkaloids have been obtained only in methanol. |
| 收录类别 | SCI |
| 语种 | 英语 |
| WOS记录号 | WOS:000254348700007 |
| 公开日期 | 2010-04-14 |
| 源URL | [http://ir.ciac.jl.cn/handle/322003/10621]  |
| 专题 | 长春应用化学研究所_长春应用化学研究所知识产出_期刊论文 |
| 推荐引用方式 GB/T 7714 | Yue H,Pi ZF,Li HL,et al. Studies on the stability of diester-diterpenoid alkaloids from the genus Aconitum L. by high performance liquid chromatography combined with electrospray ionisation tandem mass spectrometry (HPLC/ESI/MSn)[J]. phytochemical analysis,2008,19(2):141-147. |
| APA | Yue H,Pi ZF,Li HL,Song FR,Liu ZQ,&Liu SY.(2008).Studies on the stability of diester-diterpenoid alkaloids from the genus Aconitum L. by high performance liquid chromatography combined with electrospray ionisation tandem mass spectrometry (HPLC/ESI/MSn).phytochemical analysis,19(2),141-147. |
| MLA | Yue H,et al."Studies on the stability of diester-diterpenoid alkaloids from the genus Aconitum L. by high performance liquid chromatography combined with electrospray ionisation tandem mass spectrometry (HPLC/ESI/MSn)".phytochemical analysis 19.2(2008):141-147. |
入库方式： OAI收割
来源：长春应用化学研究所
浏览0
下载0
收藏0
其他版本
除非特别说明，本系统中所有内容都受版权保护，并保留所有权利。