中国科学院机构知识库网格
Chinese Academy of Sciences Institutional Repositories Grid
GIUSAXS and AFM Studies on Surface Reconstruction of Latex Thin Films during Thermal Treatment

文献类型:期刊论文

作者Hu SS ; Rieger J ; Roth SV ; Gehrke R ; Leyrer RJ ; Men YF
刊名langmuir
出版日期2009
卷号25期号:7页码:4230-4234
关键词X-RAY-SCATTERING ATOMIC-FORCE MICROSCOPY IN-SITU GISAXS GRAZING-INCIDENCE COALESCENCE CRYSTALS
ISSN号0743-7463
通讯作者men yf
中文摘要the structural evolution of a single-layer latex film during annealing was studied via grazing incidence ultrasmall-angle x-ray scattering (giusaxs) and atomic force microscopy (afm). the latex particles were composed of a low-t-g (-54 degrees c) core (n-butylacrylate, 30 wt %) and a high-t-g (41 degrees c) shell (t-butylacrylate, 70 wt %) and had an overall diameter of about 500 nm. giusaxs data indicate that the q(y) scan at q(z) = 0.27 nm(-1) (out-of-plane scan) contains information about both the structure factor and the form factor. the giusaxs data on latex films annealed at various temperatures ranging from room temperature to 140 degrees c indicate that the structure of the latex thin film beneath the surface changed significantly. the evolution of the out-of-plane scan plot reveals the surface reconstruction of the film. furthermore, we also followed the time-dependent behavior of structural evolution when the latex film was annealed at a relatively low temperature (60 degrees c) where restructuring within the film can be followed that cannot be detected by afm, which detects only surface morphology.
收录类别SCI
语种英语
WOS记录号WOS:000264798000041
公开日期2010-05-04
源URL[http://202.98.16.49/handle/322003/11801]  
专题长春应用化学研究所_长春应用化学研究所知识产出_期刊论文
推荐引用方式
GB/T 7714
Hu SS,Rieger J,Roth SV,et al. GIUSAXS and AFM Studies on Surface Reconstruction of Latex Thin Films during Thermal Treatment[J]. langmuir,2009,25(7):4230-4234.
APA Hu SS,Rieger J,Roth SV,Gehrke R,Leyrer RJ,&Men YF.(2009).GIUSAXS and AFM Studies on Surface Reconstruction of Latex Thin Films during Thermal Treatment.langmuir,25(7),4230-4234.
MLA Hu SS,et al."GIUSAXS and AFM Studies on Surface Reconstruction of Latex Thin Films during Thermal Treatment".langmuir 25.7(2009):4230-4234.

入库方式: OAI收割

来源:长春应用化学研究所

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