GIUSAXS and AFM Studies on Surface Reconstruction of Latex Thin Films during Thermal Treatment
文献类型:期刊论文
作者 | Hu SS ; Rieger J ; Roth SV ; Gehrke R ; Leyrer RJ ; Men YF |
刊名 | langmuir
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出版日期 | 2009 |
卷号 | 25期号:7页码:4230-4234 |
关键词 | X-RAY-SCATTERING ATOMIC-FORCE MICROSCOPY IN-SITU GISAXS GRAZING-INCIDENCE COALESCENCE CRYSTALS |
ISSN号 | 0743-7463 |
通讯作者 | men yf |
中文摘要 | the structural evolution of a single-layer latex film during annealing was studied via grazing incidence ultrasmall-angle x-ray scattering (giusaxs) and atomic force microscopy (afm). the latex particles were composed of a low-t-g (-54 degrees c) core (n-butylacrylate, 30 wt %) and a high-t-g (41 degrees c) shell (t-butylacrylate, 70 wt %) and had an overall diameter of about 500 nm. giusaxs data indicate that the q(y) scan at q(z) = 0.27 nm(-1) (out-of-plane scan) contains information about both the structure factor and the form factor. the giusaxs data on latex films annealed at various temperatures ranging from room temperature to 140 degrees c indicate that the structure of the latex thin film beneath the surface changed significantly. the evolution of the out-of-plane scan plot reveals the surface reconstruction of the film. furthermore, we also followed the time-dependent behavior of structural evolution when the latex film was annealed at a relatively low temperature (60 degrees c) where restructuring within the film can be followed that cannot be detected by afm, which detects only surface morphology. |
收录类别 | SCI |
语种 | 英语 |
WOS记录号 | WOS:000264798000041 |
公开日期 | 2010-05-04 |
源URL | [http://202.98.16.49/handle/322003/11801] ![]() |
专题 | 长春应用化学研究所_长春应用化学研究所知识产出_期刊论文 |
推荐引用方式 GB/T 7714 | Hu SS,Rieger J,Roth SV,et al. GIUSAXS and AFM Studies on Surface Reconstruction of Latex Thin Films during Thermal Treatment[J]. langmuir,2009,25(7):4230-4234. |
APA | Hu SS,Rieger J,Roth SV,Gehrke R,Leyrer RJ,&Men YF.(2009).GIUSAXS and AFM Studies on Surface Reconstruction of Latex Thin Films during Thermal Treatment.langmuir,25(7),4230-4234. |
MLA | Hu SS,et al."GIUSAXS and AFM Studies on Surface Reconstruction of Latex Thin Films during Thermal Treatment".langmuir 25.7(2009):4230-4234. |
入库方式: OAI收割
来源:长春应用化学研究所
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