Direct Analysis of Succinic Acid Fermentation Broth by H-1 Diffusion-Ordered NMR Spectroscopy and Quantitative H-1 NMR Technique
文献类型：期刊论文
| 作者 | Wang, Limin2; Yang, Ying1 ; Yang, Haiyan1; Qiu, Ruchen2; Huang, Shaohua1
|
| 刊名 | ACS SUSTAINABLE CHEMISTRY & ENGINEERING
 |
| 出版日期 | 2017-04-01 |
| 卷号 | 5期号:4页码:2824-2828 |
| 关键词 | Succinic acid fermentation broth Diffusion-ordered NMR spectroscopy Quantitative H-1 NMR technique Qualitative analysis Quantitative analysis |
| 英文摘要 | The diffusion-ordered NMR spectroscopy (DOSY) protocol was first introduced to analyze directly the mixture samples of succinic acid fermentation broth. The NMR signals of the model mixtures and the practical mixture were facilely separated, and each component was fully assigned in the diffusion dimension of DOSY spectra. The composition of succinic acid fermentation broth could be rapidly determined according to the DOSY experiments. In contrast, this qualitative analysis could not be implemented through ion chromatography technique. On the basis of DOSY experimental results, the quantitative H-1 NMR (qHNMR) technique was further used to determinate successfully the components of one mixture sample of practical fermentation broth, which agreed well with the high-performance liquid chromatographic experimental result. The quantitative analysis results demonstrate that the DOSY technique and the qHNMR technique can determination of the product quality of succinic acid fermentation broth. |
| WOS标题词 | Science & Technology ; Physical Sciences ; Technology |
| 类目[WOS] | Chemistry, Multidisciplinary ; Engineering, Chemical |
| 研究领域[WOS] | Chemistry ; Engineering |
| 关键词[WOS] | RENEWABLE RESOURCES ; MATRIX |
| 收录类别 | SCI |
| 语种 | 英语 |
| WOS记录号 | WOS:000398429700005 |
| 源URL | [http://ir.qibebt.ac.cn/handle/337004/9294]  |
| 专题 | 青岛生物能源与过程研究所_条件保障部公共实验室 |
| 作者单位 | 1.Chinese Acad Sci, Qingdao Inst Bioenergy & Bioproc Technol, Shandong Prov Key Lab Synthet Biol, 189 Songling Rd, Qingdao 266101, Peoples R China 2.Qingdao Univ Sci & Technol, Coll Chem Engn, 53 Zhengzhou Rd, Qingdao 266042, Peoples R China |
| 推荐引用方式 GB/T 7714 | Wang, Limin,Yang, Ying,Yang, Haiyan,et al. Direct Analysis of Succinic Acid Fermentation Broth by H-1 Diffusion-Ordered NMR Spectroscopy and Quantitative H-1 NMR Technique[J]. ACS SUSTAINABLE CHEMISTRY & ENGINEERING,2017,5(4):2824-2828. |
| APA | Wang, Limin,Yang, Ying,Yang, Haiyan,Qiu, Ruchen,&Huang, Shaohua.(2017).Direct Analysis of Succinic Acid Fermentation Broth by H-1 Diffusion-Ordered NMR Spectroscopy and Quantitative H-1 NMR Technique.ACS SUSTAINABLE CHEMISTRY & ENGINEERING,5(4),2824-2828. |
| MLA | Wang, Limin,et al."Direct Analysis of Succinic Acid Fermentation Broth by H-1 Diffusion-Ordered NMR Spectroscopy and Quantitative H-1 NMR Technique".ACS SUSTAINABLE CHEMISTRY & ENGINEERING 5.4(2017):2824-2828. |
入库方式： OAI收割
来源：青岛生物能源与过程研究所
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