Studies on lignan constituents from Schisandra chinensis (Turcz.) Baill. fruits using high-performance liquid chromatography/electrospray ionization multiple-stage tandem mass spectrometry
文献类型：期刊论文
| 作者 | Huang X ; Song FR ; Liu ZQ ; Liu SY |
| 刊名 | journal of mass spectrometry
 |
| 出版日期 | 2007 |
| 卷号 | 42期号:9页码:1148-1161 |
| 关键词 | ELECTROKINETIC CAPILLARY CHROMATOGRAPHY COUNTER-CURRENT CHROMATOGRAPHY SCHIZANDRA-CHINENSIS ALKALOIDS SEPARATION GOMISIN SEEDS SAPONINS HERBS MS |
| ISSN号 | 1076-5174 |
| 通讯作者 | liu sy |
| 中文摘要 | a reversed-phase high-performance liquid chromatography-diode array detector-electrospray ionization multiple-stage tandem mass spectrometry (rp-hplc-dad-esl-msn) method has been developed for the detection and analysis of lignan constituents in the methanol extract from the fruits of schisandra chinensis (turcz.) baill. rp-hplc-dad-esi-msn and electrospray ionization fourier transform ion cyclotron resonance multiple-stage tandem mass spectrometry (esi-ft-tcr-msn) have been applied to investigate the characteristic product ions of four lignan reference compounds. then, the logical fragmentation pathways of the lignans have been proposed. by comparing the retention time (t(r)) of hplc, the esi-msn data and the structures of analyzed compounds with the data of reference compounds and in the literature, 11 peaks in hplc have been unambiguously identified and another 5 peaks have been tentatively identified or deduced. also, in the present paper, the extracted ion chromatograms (eic) have been used to analyze the lignan isomers. the experimental results demonstrate that rp-hplc-dad-esi-msn is a specific and useful method for the identification of the lignan constituents and their isomers. |
| 收录类别 | SCI |
| 语种 | 英语 |
| WOS记录号 | WOS:000249463000003 |
| 公开日期 | 2010-07-13 |
| 源URL | [http://ir.ciac.jl.cn/handle/322003/13321]  |
| 专题 | 长春应用化学研究所_长春应用化学研究所知识产出_期刊论文 |
| 推荐引用方式 GB/T 7714 | Huang X,Song FR,Liu ZQ,et al. Studies on lignan constituents from Schisandra chinensis (Turcz.) Baill. fruits using high-performance liquid chromatography/electrospray ionization multiple-stage tandem mass spectrometry[J]. journal of mass spectrometry,2007,42(9):1148-1161. |
| APA | Huang X,Song FR,Liu ZQ,&Liu SY.(2007).Studies on lignan constituents from Schisandra chinensis (Turcz.) Baill. fruits using high-performance liquid chromatography/electrospray ionization multiple-stage tandem mass spectrometry.journal of mass spectrometry,42(9),1148-1161. |
| MLA | Huang X,et al."Studies on lignan constituents from Schisandra chinensis (Turcz.) Baill. fruits using high-performance liquid chromatography/electrospray ionization multiple-stage tandem mass spectrometry".journal of mass spectrometry 42.9(2007):1148-1161. |
入库方式： OAI收割
来源：长春应用化学研究所
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