One-pot synthesis of substituted isothiazol-3(2H)-ones: Intramolecular annulation of alpha-carbamoyl ketene-S,S-acetals via PIFA-Mediated N-S bond formation
文献类型:期刊论文
作者 | Huang J ; Lu YM ; Qiu BF ; Liang YJ ; Li N ; Dong DW |
刊名 | synthesis-stuttgart
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出版日期 | 2007 |
期号 | 18页码:2791-2796 |
关键词 | HYPERVALENT IODINE(III) REAGENT FACILE SYNTHESIS 1 PRACTICAL SYNTHESIS ACYLNITRENIUM IONS STRATEGY CYCLIZATION DIRECTIONS INHIBITORS CHEMISTRY 2-BENZISOTHIAZOLE DERIVATIVES |
ISSN号 | 0039-7881 |
通讯作者 | dong dw |
中文摘要 | a facile and efficient synthetic route towards; highly substituted isothiazol-3(2h)-ones 2 from readily available u.-carbamoyl ketene-s,s-acetals 1 is presented. the key step features the formation of an n-acylnitrenium ion, generated from the oxidization of substituted amides with the hypervalent iodine reagent phenyliodine(iii) bis(trifluoroacetate) (pifa), and its succeeding intramolecular amidation to form a new n-s bond affording the title compounds. |
收录类别 | SCI |
语种 | 英语 |
WOS记录号 | WOS:000250008600004 |
公开日期 | 2010-07-13 |
源URL | [http://ir.ciac.jl.cn/handle/322003/14323] ![]() |
专题 | 长春应用化学研究所_长春应用化学研究所知识产出_期刊论文 |
推荐引用方式 GB/T 7714 | Huang J,Lu YM,Qiu BF,et al. One-pot synthesis of substituted isothiazol-3(2H)-ones: Intramolecular annulation of alpha-carbamoyl ketene-S,S-acetals via PIFA-Mediated N-S bond formation[J]. synthesis-stuttgart,2007(18):2791-2796. |
APA | Huang J,Lu YM,Qiu BF,Liang YJ,Li N,&Dong DW.(2007).One-pot synthesis of substituted isothiazol-3(2H)-ones: Intramolecular annulation of alpha-carbamoyl ketene-S,S-acetals via PIFA-Mediated N-S bond formation.synthesis-stuttgart(18),2791-2796. |
MLA | Huang J,et al."One-pot synthesis of substituted isothiazol-3(2H)-ones: Intramolecular annulation of alpha-carbamoyl ketene-S,S-acetals via PIFA-Mediated N-S bond formation".synthesis-stuttgart .18(2007):2791-2796. |
入库方式: OAI收割
来源:长春应用化学研究所
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