Study of the mechanism of nanocrystalline Pb(Zr0.52Ti0.48)O-3 prepared by accelerated sol-gel process
文献类型:期刊论文
作者 | Guo HX ; Liu YY ; Dou BS ; Xia HK |
刊名 | integrated ferroelectrics
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出版日期 | 2004 |
卷号 | 62页码:89-95 |
ISSN号 | 1058-4587 |
通讯作者 | guo hx |
中文摘要 | nanocrystalline pb(zr0.52ti0.48)o-3 was prepared from lead acetate, zirconium oxynitrate and titanium tetra-n-butoxide by a sol-gel method. it is found that both the crystallization temperature of precursor pzt and pzt product size were increased with increase of v(c3h8o2)/v(h2o) ratio in solution used. at v(c3h8o2)/v(h2o) = 4.47 the gel was formed moderately quick, and the nanocrystalline pzt with uniform granularity and low crystallizing temperature could be obtained. the diameter of the final nanocrystalline was ranged 60similar to70 nm as measured by atomic force microscopy (afm). the crystallizing temperature of the precursor pzt was 443degreesc and the crystallization reaction was completed at 500degreesc by dta and tg. the sol-gel reaction process was monitored by ft-ir and xrd. |
收录类别 | SCI |
语种 | 英语 |
WOS记录号 | WOS:000222470800014 |
公开日期 | 2010-08-17 |
源URL | [http://202.98.16.49/handle/322003/14739] ![]() |
专题 | 长春应用化学研究所_长春应用化学研究所知识产出_期刊论文 |
推荐引用方式 GB/T 7714 | Guo HX,Liu YY,Dou BS,et al. Study of the mechanism of nanocrystalline Pb(Zr0.52Ti0.48)O-3 prepared by accelerated sol-gel process[J]. integrated ferroelectrics,2004,62:89-95. |
APA | Guo HX,Liu YY,Dou BS,&Xia HK.(2004).Study of the mechanism of nanocrystalline Pb(Zr0.52Ti0.48)O-3 prepared by accelerated sol-gel process.integrated ferroelectrics,62,89-95. |
MLA | Guo HX,et al."Study of the mechanism of nanocrystalline Pb(Zr0.52Ti0.48)O-3 prepared by accelerated sol-gel process".integrated ferroelectrics 62(2004):89-95. |
入库方式: OAI收割
来源:长春应用化学研究所
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