Determination of Hg(II) in waters by on-line preconcentration using Cyanex 923 as a sorbent - Cold vapor atomic absorption spectrometry
文献类型：期刊论文
| 作者 | Duan TC ; Song XJ ; Xu JW ; Guo PR ; Chen HT ; Li HF |
| 刊名 | spectrochimica acta part b-atomic spectroscopy
 |
| 出版日期 | 2006 |
| 卷号 | 61期号:9页码:1069-1073 |
| 关键词 | LIQUID-LIQUID-EXTRACTION ANION-EXCHANGE RESIN EMISSION-SPECTROMETRY INORGANIC MERCURY NATURAL-WATERS SEA-WATER SEPARATION SAMPLES CHROMATOGRAPHY METHYLMERCURY |
| ISSN号 | 0584-8547 |
| 通讯作者 | chen ht |
| 中文摘要 | using a solid phase extraction mini-column home-made from a neutral extractant cyanex 923, inorganic hg could be on-line preconcentrated and simultaneously separated from methyl mercury. the preconcentrated hg (11) was then eluted with 10% hno3 and subsequently reduced by nabh4 to form hg vapor before determination by cold vapor atomic absorption spectrometry (cvaas). optimal conditions for and interferences on the hg preconcentration and measurement were at 1% hcl, for a 25 ml sample uptake volume and a 10 ml min(-1) sample loading rate. the detection limit was 0.2 ng l-1 and much lower than that of conventional method (around 15.8 ng l-1). the relative standard deviation (rsd) is 1.8% for measurements of 40 ng l-1 of hg and the linear working curve is from 20 to 2000 ng l-1 (with a correlation coefficient of 0.9996). the method was applied in determination of inorganic hg in city lake and deep well water (from changchun, jilin, china), and recovery test results for both samples were satisfactory. |
| 收录类别 | SCI |
| 语种 | 英语 |
| WOS记录号 | WOS:000243091100009 |
| 公开日期 | 2010-08-17 |
| 源URL | [http://ir.ciac.jl.cn/handle/322003/16343]  |
| 专题 | 长春应用化学研究所_长春应用化学研究所知识产出_期刊论文 |
| 推荐引用方式 GB/T 7714 | Duan TC,Song XJ,Xu JW,et al. Determination of Hg(II) in waters by on-line preconcentration using Cyanex 923 as a sorbent - Cold vapor atomic absorption spectrometry[J]. spectrochimica acta part b-atomic spectroscopy,2006,61(9):1069-1073. |
| APA | Duan TC,Song XJ,Xu JW,Guo PR,Chen HT,&Li HF.(2006).Determination of Hg(II) in waters by on-line preconcentration using Cyanex 923 as a sorbent - Cold vapor atomic absorption spectrometry.spectrochimica acta part b-atomic spectroscopy,61(9),1069-1073. |
| MLA | Duan TC,et al."Determination of Hg(II) in waters by on-line preconcentration using Cyanex 923 as a sorbent - Cold vapor atomic absorption spectrometry".spectrochimica acta part b-atomic spectroscopy 61.9(2006):1069-1073. |
入库方式： OAI收割
来源：长春应用化学研究所
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