中国科学院机构知识库网格
Chinese Academy of Sciences Institutional Repositories Grid
Determination of Nb and Ta in Nb/Ta minerals by inductively coupled plasmas optical emission spectrometry using slurry sample introduction

文献类型:期刊论文

作者Song XJ ; Duan TC ; Guo PR ; Chen HT
刊名microchemical journal
出版日期2006
卷号84期号:1-2页码:22-25
关键词GEOLOGICAL SAMPLES LASER-ABLATION ICP-MS NEBULIZATION IMPURITIES NITRIDE SOLIDS
ISSN号0026-265x
通讯作者chen ht
中文摘要the determination of nb and ta in nb-ta minerals was accomplished by slurry nebulization inductively coupled plasma optical emission spectrometry (icp-oes), using a clog-free v-groove ceramic nebulizer. samples were first wet-ground to appropriate particle sizes with narrow size distribution and 90% of the particles in the slurry were smaller than 2.32 mu m in diameter. subsamples were then dispersed in ph 9 aqueous solutions, and agitated in an ultrasonic bath for 15 min prior to analysis. due to the lack of slurry standards matching well with the samples, calibration was simply carried out using aqueous solution standards. results were compared with those obtained from a conventional fusion decomposition procedure and acid digestion procedures and a good agreement between the measured and referred values was obtained. the technique provided a good alternative for the rapid determination of nb and/or ta in their corresponding minerals.
收录类别SCI
语种英语
WOS记录号WOS:000240428800004
公开日期2010-08-17
源URL[http://ir.ciac.jl.cn/handle/322003/16523]  
专题长春应用化学研究所_长春应用化学研究所知识产出_期刊论文
推荐引用方式
GB/T 7714
Song XJ,Duan TC,Guo PR,et al. Determination of Nb and Ta in Nb/Ta minerals by inductively coupled plasmas optical emission spectrometry using slurry sample introduction[J]. microchemical journal,2006,84(1-2):22-25.
APA Song XJ,Duan TC,Guo PR,&Chen HT.(2006).Determination of Nb and Ta in Nb/Ta minerals by inductively coupled plasmas optical emission spectrometry using slurry sample introduction.microchemical journal,84(1-2),22-25.
MLA Song XJ,et al."Determination of Nb and Ta in Nb/Ta minerals by inductively coupled plasmas optical emission spectrometry using slurry sample introduction".microchemical journal 84.1-2(2006):22-25.

入库方式: OAI收割

来源:长春应用化学研究所

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