Capillary electrophoresis with electrochemiluminescence detection of procyclidine in human urine pretreated by ion-exchange cartridge
文献类型：期刊论文
| 作者 | Sun XH ; Liu JF ; Cao WD ; Yang XR ; Wang EK ; Fung YS |
| 刊名 | analytica chimica acta
 |
| 出版日期 | 2002 |
| 卷号 | 470期号:2页码:137-145 |
| 关键词 | RU(BPY)(3)(3+)-BASED CHEMILUMINESCENCE DETECTION AMINO-ACIDS LIQUID-CHROMATOGRAPHY TRIS(2 2'-BIPYRIDINE)RUTHENIUM(III) |
| ISSN号 | 0003-2670 |
| 通讯作者 | wang ek |
| 中文摘要 | this paper describe a ru(bpy)(3)(2+) based electrochemiluminescence (ecl) method to detect procyclidine in human urine following separation by capillary electrophoresis (ce). an ecl detection cell was designed for post-column addition of ru(bpy)(3)(2+). parameters affecting separation and detection were optimized, leading to a detection limit of 1 x 10(-9) mol/l in an on-capillary stacking mode. for application in urine, a cartridge packed with slightly acidic cation-exchange resin was used to eliminate the matrix effects of urine and improve the detection sensitivity. extraction recovery was nearly 90%. |
| 收录类别 | SCI收录期刊论文 |
| 语种 | 英语 |
| WOS记录号 | WOS:000178666000004 |
| 公开日期 | 2010-11-03 |
| 源URL | [http://202.98.16.49/handle/322003/18291]  |
| 专题 | 长春应用化学研究所_长春应用化学研究所知识产出_期刊论文 |
| 推荐引用方式 GB/T 7714 | Sun XH,Liu JF,Cao WD,et al. Capillary electrophoresis with electrochemiluminescence detection of procyclidine in human urine pretreated by ion-exchange cartridge[J]. analytica chimica acta,2002,470(2):137-145. |
| APA | Sun XH,Liu JF,Cao WD,Yang XR,Wang EK,&Fung YS.(2002).Capillary electrophoresis with electrochemiluminescence detection of procyclidine in human urine pretreated by ion-exchange cartridge.analytica chimica acta,470(2),137-145. |
| MLA | Sun XH,et al."Capillary electrophoresis with electrochemiluminescence detection of procyclidine in human urine pretreated by ion-exchange cartridge".analytica chimica acta 470.2(2002):137-145. |
入库方式： OAI收割
来源：长春应用化学研究所
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