中国科学院机构知识库网格
Chinese Academy of Sciences Institutional Repositories Grid
Microstructure analysis of nylon 66 by WAXD and SAXS

文献类型:期刊论文

作者Zhang QX ; Fu PP ; Zhang HF ; Mo ZS
刊名chemical research in chinese universities
出版日期2002
卷号18期号:3页码:358-363
关键词COMPOSITES CRYSTALLIZATION POLYETHYLENE INTERPHASE POLYMERS CARBON
ISSN号1005-9040
中文摘要the analysis of the small angle x-ray scattering (saxs) data was based upon particle characteristic function, one-dimensional electron-density correlation function and particle distribution function. the microstructure of nylon 66 with different degrees of crystallinity was studied by means of x-ray scattering method. the radius of gyration r-g, the porod radius r-p, the thickness of crystalline region l-c the thickness of non-crystalline region l-n, the thickness of interphase region d(tr), the long period l, the semiaxises of particles (a, a, b), the distribution of the particle sizes and the scattering invariant were calculated. the results indicate that there was a significant interphase region between the crystalline region and the non-crystalline region. and its content (w-t,w-x) should not be neglected in comparison with that of crystalline region w-c,w-x. the morphology of nylon 66 prepared by isothermal crystallization at a high temperature was mainly a lamellar structure, while the spherical crystals dominated in the quenched sample. the size of the particles in the quenched sample was smaller than that of those in the isothermally crystallized sample. and the distribution of the particle sizes in the isothermally crystallized sample was wider.
收录类别SCI收录期刊论文
语种英语
WOS记录号WOS:000177704500033
公开日期2010-11-03
源URL[http://202.98.16.49/handle/322003/18355]  
专题长春应用化学研究所_长春应用化学研究所知识产出_期刊论文
推荐引用方式
GB/T 7714
Zhang QX,Fu PP,Zhang HF,et al. Microstructure analysis of nylon 66 by WAXD and SAXS[J]. chemical research in chinese universities,2002,18(3):358-363.
APA Zhang QX,Fu PP,Zhang HF,&Mo ZS.(2002).Microstructure analysis of nylon 66 by WAXD and SAXS.chemical research in chinese universities,18(3),358-363.
MLA Zhang QX,et al."Microstructure analysis of nylon 66 by WAXD and SAXS".chemical research in chinese universities 18.3(2002):358-363.

入库方式: OAI收割

来源:长春应用化学研究所

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