Determination of propranolol by capillary electrophoresis with end-column amperometric detection
文献类型:期刊论文
作者 | Bai XX ; You TY ; Sun HW ; Yang XR ; Wang EK |
刊名 | electroanalysis
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出版日期 | 2000 |
卷号 | 12期号:7页码:535-537 |
关键词 | IMPROVED CHIRAL SEPARATION GAS-CHROMATOGRAPHY BETA-BLOCKERS ATENOLOL CYCLODEXTRIN SPECTROMETRY METOPROLOL REAGENTS |
ISSN号 | 1040-0397 |
通讯作者 | yang xr |
中文摘要 | a capillary electrophoresis-amperometric detection system was developed for the determination of propranolol (pro) at a 33 mu m carbon fiber microdisk electrode (cfe). the cyclic voltammogram, the hydrodynamic voltammograms and the effect of ph were studied. under the optimum conditions: separation voltage 15 kv; injection 3 s at 15 kv; 10 mm ph 7.5 phosphate buffer, 1.15 v (vs. ag/agcl) detection potential, the detection limit (lod) for pro was 0.05 mu m (s/n = 3). the response for pro was linear over two orders of magnitude with a linear correlation coefficient of 0.994. the feasibility of this method was demonstrated by the detection of pro in urine sample. |
收录类别 | SCI收录期刊论文 |
语种 | 英语 |
WOS记录号 | WOS:000087138100012 |
公开日期 | 2010-11-04 |
源URL | [http://202.98.16.49/handle/322003/19745] ![]() |
专题 | 长春应用化学研究所_长春应用化学研究所知识产出_期刊论文 |
推荐引用方式 GB/T 7714 | Bai XX,You TY,Sun HW,et al. Determination of propranolol by capillary electrophoresis with end-column amperometric detection[J]. electroanalysis,2000,12(7):535-537. |
APA | Bai XX,You TY,Sun HW,Yang XR,&Wang EK.(2000).Determination of propranolol by capillary electrophoresis with end-column amperometric detection.electroanalysis,12(7),535-537. |
MLA | Bai XX,et al."Determination of propranolol by capillary electrophoresis with end-column amperometric detection".electroanalysis 12.7(2000):535-537. |
入库方式: OAI收割
来源:长春应用化学研究所
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