DETERMINATION OF AMINOPYRINE AND ITS METABOLITE IN BIOLOGICAL FLUID BY LIQUID-CHROMATOGRAPHY ELECTROCHEMISTRY WITH A GLASSY-CARBON ELECTRODE DISPERSED WITH ALPHA-ALUMINA PARTICLES
文献类型：期刊论文
| 作者 | LI HM ; WANG E |
| 刊名 | electroanalysis
 |
| 出版日期 | 1995 |
| 卷号 | 7期号:3页码:280-282 |
| ISSN号 | 1040-0397 |
| 通讯作者 | li hm |
| 中文摘要 | a sensitive high-performance liquid chromatographic method has been developed for the quantitative determination of aminopyrine (am) and its metabolite 4-aminoantipyrine (aan). the method utilizes reverse-phase chromatography/amperometric detection with a glassy carbon electrode dispersed with alpha-arumina particles as the working electrode, on which the oxidation of am and aan was greatly improved compared with that on a bare glassy carbon electrode. as a result, the detection limit was as low as 1.4 ng for am and 0.8 ng for aan, and the calibration plots for the above compounds have wide linear ranges from 100 ng/ml to 100 mu g/ml and 60 ng/ml to 80 mu g/ml (for am and aan, respectively). the above method was applied for the detection of these materials in human urine with satisfactory results. |
| 收录类别 | SCI收录期刊论文 |
| 语种 | 英语 |
| 公开日期 | 2010-12-30 ; 2011-06-10 |
| 源URL | [http://ir.ciac.jl.cn/handle/322003/26641]  |
| 专题 | 长春应用化学研究所_长春应用化学研究所知识产出_期刊论文 |
| 推荐引用方式 GB/T 7714 | LI HM,WANG E. DETERMINATION OF AMINOPYRINE AND ITS METABOLITE IN BIOLOGICAL FLUID BY LIQUID-CHROMATOGRAPHY ELECTROCHEMISTRY WITH A GLASSY-CARBON ELECTRODE DISPERSED WITH ALPHA-ALUMINA PARTICLES[J]. electroanalysis,1995,7(3):280-282. |
| APA | LI HM,&WANG E.(1995).DETERMINATION OF AMINOPYRINE AND ITS METABOLITE IN BIOLOGICAL FLUID BY LIQUID-CHROMATOGRAPHY ELECTROCHEMISTRY WITH A GLASSY-CARBON ELECTRODE DISPERSED WITH ALPHA-ALUMINA PARTICLES.electroanalysis,7(3),280-282. |
| MLA | LI HM,et al."DETERMINATION OF AMINOPYRINE AND ITS METABOLITE IN BIOLOGICAL FLUID BY LIQUID-CHROMATOGRAPHY ELECTROCHEMISTRY WITH A GLASSY-CARBON ELECTRODE DISPERSED WITH ALPHA-ALUMINA PARTICLES".electroanalysis 7.3(1995):280-282. |
入库方式： OAI收割
来源：长春应用化学研究所
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