One-step preparation of zirconia coated silica microspheres and modification with D-fructose 1, 6-bisphosphate as stationary phase for hydrophilic interaction chromatography
文献类型：期刊论文
| 作者 | Li, Shenghong1; Song, Zhihua1,2; Duan, Chunfeng1; Shi, Meng1,2; Guan, Yafeng1 |
| 刊名 | JOURNAL OF CHROMATOGRAPHY A
 |
| 出版日期 | 2017-11-03 |
| 卷号 | 1522页码:30-37 |
| 关键词 | ZrO2 coated SiO2 Surfactant-free D-Fructose 1 6-Bisphosphate Hydrophilic interaction chromatography |
| 英文摘要 | In this study, ZrO2 layer coated silica microspheres (ZrO2/SiO2) were successfully prepared by a facile one-step surfactant-free hydrothermal route under low pH condition. The synthesized ZrO2/SiO2 material was then modified with D-fructose 1, 6-bisphosphate (FDP) to improve the chromatographic separation property of the material. Fused-silica capillary columns were prepared with the modified material for evaluation. Phenolic, nucleobases and alkaloids compounds in hydrophilic interaction chromatographic (HILIC) mode showed symmetrical peaks. The FDP-ZrO2/SiO2 stationary phase showed better performance than ZrO2/SiO2 packing material and demonstrated great potential for application in HILIC mode. (C) 2017 Elsevier B.V. All rights reserved. |
| WOS标题词 | Science & Technology ; Life Sciences & Biomedicine ; Physical Sciences |
| 类目[WOS] | Biochemical Research Methods ; Chemistry, Analytical |
| 研究领域[WOS] | Biochemistry & Molecular Biology ; Chemistry |
| 关键词[WOS] | HPLC SEPARATION ; BONDED SILICA ; PERFORMANCE ; SPHERES ; NANOPARTICLES ; RETENTION |
| 收录类别 | SCI |
| 语种 | 英语 |
| WOS记录号 | WOS:000413383200005 |
| 源URL | [http://cas-ir.dicp.ac.cn/handle/321008/149767]  |
| 专题 | 大连化学物理研究所_中国科学院大连化学物理研究所 |
| 作者单位 | 1.Chinese Acad Sci, Dalian Inst Chem Phys, CAS Key Lab Separat Sci Analyt Chem, 457 Zhongshan Rd, Dalian 116023, Peoples R China 2.Univ Chinese Acad Sci, Beijing 100039, Peoples R China |
| 推荐引用方式 GB/T 7714 | Li, Shenghong,Song, Zhihua,Duan, Chunfeng,et al. One-step preparation of zirconia coated silica microspheres and modification with D-fructose 1, 6-bisphosphate as stationary phase for hydrophilic interaction chromatography[J]. JOURNAL OF CHROMATOGRAPHY A,2017,1522:30-37. |
| APA | Li, Shenghong,Song, Zhihua,Duan, Chunfeng,Shi, Meng,&Guan, Yafeng.(2017).One-step preparation of zirconia coated silica microspheres and modification with D-fructose 1, 6-bisphosphate as stationary phase for hydrophilic interaction chromatography.JOURNAL OF CHROMATOGRAPHY A,1522,30-37. |
| MLA | Li, Shenghong,et al."One-step preparation of zirconia coated silica microspheres and modification with D-fructose 1, 6-bisphosphate as stationary phase for hydrophilic interaction chromatography".JOURNAL OF CHROMATOGRAPHY A 1522(2017):30-37. |
入库方式： OAI收割
来源：大连化学物理研究所
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