Construction of an off-line two dimensional reversed-phase liquid chromatography/ultra-high performance supercritical fluid chromatography method for rapid and comprehensive analysis of Piper kadsura
文献类型：期刊论文
| 作者 | Jin, Yu2; Xin, Huaxia2; Fu, Qing2; Yuan, Yun2; Liu, Yanfang1; Ke, Yanxiong2; Liang, Xinmiao1,2 |
| 刊名 | JOURNAL OF SUPERCRITICAL FLUIDS
 |
| 出版日期 | 2017-09-01 |
| 卷号 | 127页码:9-14 |
| 关键词 | Ultra-high performance supercritical fluid chromatography Reversed-phase liquid chromatography Two-dimensional chromatography Rapid analysis Piper kadsura |
| 英文摘要 | In this study, ultra-high performance supercritical fluid chromatography(UHPSFC) was chosen to construct an off-line two dimensional chromatography with reversed-phase liquid chromatography (RPLC) for rapid and comprehensive analysis of Piper kadsura. The sample was firstly divided into a petroleum ether (PE) extract and an ethyl acetate (EA) extract, and then they were separated into 21 and 28 fractions in the first dimensional RPLC, respectively. In the second dimension, the effect of UHPSFC parameters on the analysis speed was investigated. Each PE fraction could be analyzed in 2.0min, and every EA fraction could be analyzed in 3.0 min. In total, at least 1033 peaks were detected by this method, including 204 peaks from the PE fractions and 829 peaks from the EA fractions. The 2D-RPLC/UHPSFC system with the characteristics of fast separation and high orthogonality has a great potential for the rapid and comprehensive analysis of the complex samples. (C) 2017 Elsevier B.V. All rights reserved. |
| WOS标题词 | Science & Technology ; Physical Sciences ; Technology |
| 类目[WOS] | Chemistry, Physical ; Engineering, Chemical |
| 研究领域[WOS] | Chemistry ; Engineering |
| 关键词[WOS] | SEPARATION ; NEOLIGNANS ; EXTRACT |
| 收录类别 | SCI |
| 语种 | 英语 |
| WOS记录号 | WOS:000405879400002 |
| 源URL | [http://cas-ir.dicp.ac.cn/handle/321008/151907]  |
| 专题 | 大连化学物理研究所_中国科学院大连化学物理研究所 |
| 作者单位 | 1.Chinese Acad Sci, Dalian Inst Chem Phys, Key Lab Nat Med, Key Lab Separat Sci Analyt Chem, Dalian 116023, Liaoning, Peoples R China 2.East China Univ Sci & Technol, Sch Pharm, Engn Res Ctr Pharmaceut Proc Chem, Minist Educ, Shanghai 200237, Peoples R China |
| 推荐引用方式 GB/T 7714 | Jin, Yu,Xin, Huaxia,Fu, Qing,et al. Construction of an off-line two dimensional reversed-phase liquid chromatography/ultra-high performance supercritical fluid chromatography method for rapid and comprehensive analysis of Piper kadsura[J]. JOURNAL OF SUPERCRITICAL FLUIDS,2017,127:9-14. |
| APA | Jin, Yu.,Xin, Huaxia.,Fu, Qing.,Yuan, Yun.,Liu, Yanfang.,...&Liang, Xinmiao.(2017).Construction of an off-line two dimensional reversed-phase liquid chromatography/ultra-high performance supercritical fluid chromatography method for rapid and comprehensive analysis of Piper kadsura.JOURNAL OF SUPERCRITICAL FLUIDS,127,9-14. |
| MLA | Jin, Yu,et al."Construction of an off-line two dimensional reversed-phase liquid chromatography/ultra-high performance supercritical fluid chromatography method for rapid and comprehensive analysis of Piper kadsura".JOURNAL OF SUPERCRITICAL FLUIDS 127(2017):9-14. |
入库方式： OAI收割
来源：大连化学物理研究所
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