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Encapsulation of bulky solvent molecules into the channels of aluminophosphate molecular sieve and its negative influence on the thermal stability of open-framework

文献类型：期刊论文

作者Guo, Junhui1; Deng, Feng4; Xu, Jun4; Wang, Chao4; Xu, Ruren1; Sharma, Raj Pal2,3; Yan, Wenfu1
刊名INORGANIC CHEMISTRY COMMUNICATIONS
出版日期2018-05-01
卷号91页码:67-71
关键词Hydrothermal Synthesis Solvothermal Synthesis Zeolite Aluminophosphate Molecular Sieve Thermal Stability
DOI10.1016/j.inoche.2018.03.008
文献子类Article
英文摘要Three aluminophosphate molecular sieve AlPO4-5s were synthesized using water, ethylene glycol, and triethylene glycol as solvent. The products were thoroughly characterized by powder X-ray diffraction analyses, thermogravimetric analyses, scanning electron microscope analyses, and solid-state cross polarization magic angle spinning nuclear magnetic resonance analyses. The results showed that solvothermally synthesized aluminophosphate molecular sieve AlPO4-5 from triethylene glycol was much less stable than that hydrothermally synthesized from water. Therrnogravimetric analysis and C-13 cross polarization magic angle spinning nuclear magnetic resonance analyses confirmed that the bulky solvent molecules of triethylene glycol were encapsulated within the channels of AlPO4-5 and was responsible for the significant decrease of the thermal stability of open-framework. (C) 2018 Elsevier B.V. All rights reserved.
WOS关键词SOLVOTHERMAL SYNTHESIS ; ZEOLITES ; TEMPLATE ; ALPO4-5 ; CRYSTALS ; SAPO-5 ; SILICA
WOS研究方向Chemistry
语种英语
WOS记录号WOS:000430904400012
资助机构National Natural Science Foundation of China(21571075 ; National Natural Science Foundation of China(21571075 ; National Key Research and Development Program of China(2016YFB0701100) ; National Key Research and Development Program of China(2016YFB0701100) ; 111 Project(B17020) ; 111 Project(B17020) ; 21320102001 ; 21320102001 ; 21621001) ; 21621001) ; National Natural Science Foundation of China(21571075 ; National Natural Science Foundation of China(21571075 ; National Key Research and Development Program of China(2016YFB0701100) ; National Key Research and Development Program of China(2016YFB0701100) ; 111 Project(B17020) ; 111 Project(B17020) ; 21320102001 ; 21320102001 ; 21621001) ; 21621001)
源URL[http://ir.wipm.ac.cn/handle/112942/12057]  
专题武汉物理与数学研究所_磁共振应用研究部
作者单位1.Jilin Univ, Coll Chem, State Key Lab Inorgan Synth & Preparat Chem, Changchun 130012, Jilin, Peoples R China
2.Panjab Univ, CAS, Chandigarh 160014, India
3.Panjab Univ, Dept Chem, Chandigarh 160014, India
4.Chinese Acad Sci, Wuhan Inst Phys & Math, Wuhan Ctr Magnet Resonance, State Key Lab Magnet Resonance & Atom & Mol Phys, Wuhan 430071, Hubei, Peoples R China
推荐引用方式
GB/T 7714		 Guo, Junhui,Deng, Feng,Xu, Jun,et al. Encapsulation of bulky solvent molecules into the channels of aluminophosphate molecular sieve and its negative influence on the thermal stability of open-framework[J]. INORGANIC CHEMISTRY COMMUNICATIONS,2018,91:67-71.
APA Guo, Junhui.,Deng, Feng.,Xu, Jun.,Wang, Chao.,Xu, Ruren.,...&Yan, Wenfu.(2018).Encapsulation of bulky solvent molecules into the channels of aluminophosphate molecular sieve and its negative influence on the thermal stability of open-framework.INORGANIC CHEMISTRY COMMUNICATIONS,91,67-71.
MLA Guo, Junhui,et al."Encapsulation of bulky solvent molecules into the channels of aluminophosphate molecular sieve and its negative influence on the thermal stability of open-framework".INORGANIC CHEMISTRY COMMUNICATIONS 91(2018):67-71.

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来源：武汉物理与数学研究所

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