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TEMPO-Mediated Synthesis of Tetrahydropyridinofullerenes: Reaction of [60]Fullerene with alpha-Methyl-Substituted Arylmethanamines and Aldehydes in the Presence of 4-Dimethylaminopyridine

文献类型：期刊论文

作者Li, Fa-Bao1,2; Alarmry, Khalid A.4; Asiri, Abdullah M.4; Liu, Chao-Yang3; Liu, Li1,2; Huang, Yongshun1,2; Xiang, Jun-Jun1,2; Huang, Cheng1,2; Wang, Hui-Juan3; Huang, Gang1,2
刊名JOURNAL OF ORGANIC CHEMISTRY
出版日期2018-01-05
卷号83期号:1页码:85-95
ISSN号0022-3263
DOI10.1021/acs.joc.7b02378
文献子类Article
英文摘要A series of scarce tetrahydropyridinofullerenes were synthesized by the metal-free-mediated reaction of [60]fullerene with cheap and easily available alpha-methyl-substituted arylmethanamines and aldehydes in the presence of 2,2,6,6-tetramethylpiperidine-1-oxyl (TEMPO) and 4-dimethylaminopyridine (DMAP) in moderate to good yields comparable to the previously reported data for most monoadducts. The in situ generation of azadienes played a crucial role in the successful synthesis of tetrahydropyridinofullerenes. A plausible reaction mechanism was proposed to elucidate the reaction process.
WOS关键词DIELS-ALDER REACTION ; AMINO-ACID ESTERS ; SELECTIVE FORMATION ; AROMATIC-ALDEHYDES ; MOLECULAR-OXYGEN ; FULLERENE ; C-60 ; FULLEROPYRROLIDINES ; DERIVATIVES ; CHEMISTRY
WOS研究方向Chemistry
语种英语
WOS记录号WOS:000419749500008
出版者AMER CHEMICAL SOC
资助机构National Natural Science Foundation of China(21102041 ; National Natural Science Foundation of China(21102041 ; Scientific Research Foundation of Education Commission of Hubei Province(D20161007) ; Scientific Research Foundation of Education Commission of Hubei Province(D20161007) ; Innovation and Entrepreneurship Training Program for Undergraduates of Hubei Province(201610512054) ; Innovation and Entrepreneurship Training Program for Undergraduates of Hubei Province(201610512054) ; 21671061) ; 21671061) ; National Natural Science Foundation of China(21102041 ; National Natural Science Foundation of China(21102041 ; Scientific Research Foundation of Education Commission of Hubei Province(D20161007) ; Scientific Research Foundation of Education Commission of Hubei Province(D20161007) ; Innovation and Entrepreneurship Training Program for Undergraduates of Hubei Province(201610512054) ; Innovation and Entrepreneurship Training Program for Undergraduates of Hubei Province(201610512054) ; 21671061) ; 21671061) ; National Natural Science Foundation of China(21102041 ; National Natural Science Foundation of China(21102041 ; Scientific Research Foundation of Education Commission of Hubei Province(D20161007) ; Scientific Research Foundation of Education Commission of Hubei Province(D20161007) ; Innovation and Entrepreneurship Training Program for Undergraduates of Hubei Province(201610512054) ; Innovation and Entrepreneurship Training Program for Undergraduates of Hubei Province(201610512054) ; 21671061) ; 21671061) ; National Natural Science Foundation of China(21102041 ; National Natural Science Foundation of China(21102041 ; Scientific Research Foundation of Education Commission of Hubei Province(D20161007) ; Scientific Research Foundation of Education Commission of Hubei Province(D20161007) ; Innovation and Entrepreneurship Training Program for Undergraduates of Hubei Province(201610512054) ; Innovation and Entrepreneurship Training Program for Undergraduates of Hubei Province(201610512054) ; 21671061) ; 21671061)
源URL[http://ir.wipm.ac.cn/handle/112942/12790]  
专题中国科学院武汉物理与数学研究所
通讯作者Li, Fa-Bao; Liu, Chao-Yang; Liu, Li
作者单位1.Hubei Univ, Hubei Collaborat Innovat Ctr Adv Organ Chem Mat, Key Lab Synth & Applicat Organ Funct Mol,Minist, Key Lab Green Preparat & Applicat Funct Mat, Wuhan 430062, Hubei, Peoples R China
2.Hubei Univ, Sch Chem & Chem Engn, Wuhan 430062, Hubei, Peoples R China
3.Chinese Acad Sci, Wuhan Ctr Magnet Resonance, Wuhan Inst Phys & Math, State Key Lab Magnet Resonance & Atom & Mol Phys, Wuhan 430071, Hubei, Peoples R China
4.King Abdulaziz Univ, Fac Sci, Dept Chem, Jeddah 21589, Saudi Arabia
推荐引用方式
GB/T 7714		 Li, Fa-Bao,Alarmry, Khalid A.,Asiri, Abdullah M.,et al. TEMPO-Mediated Synthesis of Tetrahydropyridinofullerenes: Reaction of [60]Fullerene with alpha-Methyl-Substituted Arylmethanamines and Aldehydes in the Presence of 4-Dimethylaminopyridine[J]. JOURNAL OF ORGANIC CHEMISTRY,2018,83(1):85-95.
APA Li, Fa-Bao.,Alarmry, Khalid A..,Asiri, Abdullah M..,Liu, Chao-Yang.,Liu, Li.,...&Peng, Jie.(2018).TEMPO-Mediated Synthesis of Tetrahydropyridinofullerenes: Reaction of [60]Fullerene with alpha-Methyl-Substituted Arylmethanamines and Aldehydes in the Presence of 4-Dimethylaminopyridine.JOURNAL OF ORGANIC CHEMISTRY,83(1),85-95.
MLA Li, Fa-Bao,et al."TEMPO-Mediated Synthesis of Tetrahydropyridinofullerenes: Reaction of [60]Fullerene with alpha-Methyl-Substituted Arylmethanamines and Aldehydes in the Presence of 4-Dimethylaminopyridine".JOURNAL OF ORGANIC CHEMISTRY 83.1(2018):85-95.

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