Synthesis of Calcium Chloroborate Whiskers Via Sedimentation and Sintering Process
文献类型：期刊论文
| 作者 | Zhu Donghai1,2; Nai Xueying2 ; Lan Shengjie1,3; Dang Li1,3; Liu Xin2; Li Wu2
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| 刊名 | JOURNAL OF WUHAN UNIVERSITY OF TECHNOLOGY-MATERIALS SCIENCE EDITION
 |
| 出版日期 | 2017-10-01 |
| 卷号 | 32期号:5页码:1067-1071 |
| 关键词 | Single Crystal Growth Ca2b5o9cl Whiskers Microstructures |
| 文献子类 | Article |
| 英文摘要 | Single crystalline calcium chloroborate (Ca2B5O9Cl) whiskers with uniform diameter have been fabricated by a two-step process. The precursor was firstly prepared by the sedimentation reaction between CaCl2, H3BO3 and NaOH aqueous solutions, and then sintered at different temperatures for 6 h with KCl as flux. The XRD indicates that the product synthesized at 600 degrees C is Orthorhombic Ca2B5O9Cl. SEM and TEM results show that the Ca2B5O9Cl is whisker with the diameter about 0.2-0.5 mu m and the length up to 15 mu m. SAED analysis shows that the whisker is single crystalline and grows along [001] direction. The possible formation process and growth mechanism were proposed. |
| WOS关键词 | ALUMINUM BORATE WHISKERS ; MECHANICAL-PROPERTIES ; COMPOSITES ; BEHAVIORS |
| WOS研究方向 | Materials Science |
| 语种 | 英语 |
| WOS记录号 | WOS:000412950000013 |
| 源URL | [http://ir.isl.ac.cn/handle/363002/6261]  |
| 专题 | 青海盐湖研究所_青海盐湖研究所知识仓储 青海盐湖研究所_盐湖资源综合利用工程技术中心 |
| 作者单位 | 1.Qinghai Univ, State Key Lab Plateau Ecol & Agr, Xining 810016, Qinghai, Peoples R China 2.Chinese Acad Sci, Qinghai Inst Salt Lakes, Xining 810008, Peoples R China 3.Qinghai Univ, Sch Chem Engn, Xining 810016, Qinghai, Peoples R China |
| 推荐引用方式 GB/T 7714 | Zhu Donghai,Nai Xueying,Lan Shengjie,et al. Synthesis of Calcium Chloroborate Whiskers Via Sedimentation and Sintering Process[J]. JOURNAL OF WUHAN UNIVERSITY OF TECHNOLOGY-MATERIALS SCIENCE EDITION,2017,32(5):1067-1071. |
| APA | Zhu Donghai,Nai Xueying,Lan Shengjie,Dang Li,Liu Xin,&Li Wu.(2017).Synthesis of Calcium Chloroborate Whiskers Via Sedimentation and Sintering Process.JOURNAL OF WUHAN UNIVERSITY OF TECHNOLOGY-MATERIALS SCIENCE EDITION,32(5),1067-1071. |
| MLA | Zhu Donghai,et al."Synthesis of Calcium Chloroborate Whiskers Via Sedimentation and Sintering Process".JOURNAL OF WUHAN UNIVERSITY OF TECHNOLOGY-MATERIALS SCIENCE EDITION 32.5(2017):1067-1071. |
入库方式： OAI收割
来源：青海盐湖研究所
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