A novel silica-based column packing for reversed-phase HPLC of basic compounds
文献类型：期刊论文
| 作者 | Huang, XJ; Wang, JD; Liu, XL; Shang, ZH |
| 刊名 | chromatographia
 |
| 出版日期 | 2001-09-01 |
| 卷号 | 54期号:5-6页码:350-354 |
| 关键词 | column liquid chromatography reversed phase packing basic compounds separation |
| 英文摘要 | a novel bonded phase for reversed-phase hplc was synthesized in two steps. octylamine was first reacted with beta-(3,4-epoxycyclohexyl)ethyltrimethoxysilane (beta -ects) and then the intermediate product was coupled onto porous silica. the prepared packing was characterized by elemental analysis, solid-state c-13 nmr and fourier transform infrared (ft-ir). chromatographic evaluations were carried out by using a mixture of organic compounds including acidic, basic and neutral analytes and methanol-water as binary mobile phase. the results showed that the stationary phase has excellent chromatographic properties and is resistant to hydrolysis between ph = 2 similar to 8. it can be used efficiently for the separation of basic compounds. |
| WOS标题词 | science & technology ; life sciences & biomedicine ; physical sciences |
| 类目[WOS] | biochemical research methods ; chemistry, analytical |
| 研究领域[WOS] | biochemistry & molecular biology ; chemistry |
| 关键词[WOS] | chromatography ; performance ; polar |
| 收录类别 | SCI |
| 原文出处 | true |
| 语种 | 英语 |
| WOS记录号 | WOS:000171316600010 |
| 公开日期 | 2010-11-30 |
| 源URL | [http://159.226.238.44/handle/321008/84535]  |
| 专题 | 大连化学物理研究所_中国科学院大连化学物理研究所 |
| 作者单位 | Chinese Acad Sci, Dalian Inst Chem Phys, Dalian 116012, Peoples R China |
| 推荐引用方式 GB/T 7714 | Huang, XJ,Wang, JD,Liu, XL,et al. A novel silica-based column packing for reversed-phase HPLC of basic compounds[J]. chromatographia,2001,54(5-6):350-354. |
| APA | Huang, XJ,Wang, JD,Liu, XL,&Shang, ZH.(2001).A novel silica-based column packing for reversed-phase HPLC of basic compounds.chromatographia,54(5-6),350-354. |
| MLA | Huang, XJ,et al."A novel silica-based column packing for reversed-phase HPLC of basic compounds".chromatographia 54.5-6(2001):350-354. |
入库方式： OAI收割
来源：大连化学物理研究所
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