Fabrication of Tb3Al5O12transparent ceramics using co-precipitated nanopowders
文献类型:期刊论文
作者 | Dai, Jiawei1,2; Pan, Yubai3; Wang, Wei1; Luo, Wei1,2; Xie, Tengfei1; Kou, Huamin1; Li, Jiang1 |
刊名 | Optical Materials
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出版日期 | 2017 |
卷号 | 73页码:38-44 |
ISSN号 | 09253467 |
DOI | 10.1016/j.optmat.2017.07.047 |
英文摘要 | Terbium aluminum garnet (TAG) precursor was synthesized by a co-precipitation method from a mixed solution of terbium and aluminum nitrates using ammonium hydrogen carbonate (AHC) as the precipitant. The powders calcined at different temperatures were investigated by XRD, FTIR and FESEM in order to choose the optimal calcination temperature. Fine and low-agglomerated TAG powders with average particle size of 88 nm were obtained by calcining the precursor at 1100 °C for 4 h. Using this powder as starting material, TAG transparent ceramics were fabricated by vacuum sintering combined with hot isostatic pressing (HIP) sintering. For the sample pre-sintered at 1700 °C for 20 h with HIP post-treated at 1700 °C for 3 h, the average grain size is about 3.9 μm and the in-line transmittance is beyond 55% in the region of 500–1600 nm, reaching a maximum transmittance of 64.2% at the wavelength of 1450 nm. The Verdet constant at 633 nm is measured to be −178.9 rad T−1m−1, which is 33% larger than that of the commercial TGG single crystal (−134 rad T−1m−1). © 2017 Elsevier B.V. |
源URL | [http://ir.sic.ac.cn/handle/331005/25907] ![]() |
专题 | 中国科学院上海硅酸盐研究所 |
作者单位 | 1.Key Laboratory of Transparent Opto-functional Inorganic Materials, Shanghai Institute of Ceramics, Chinese Academy of Sciences, Shanghai; 200050, China; 2.University of Chinese Academy of Sciences, Beijing; 100049, China; 3.Department of Physics, Shanghai Normal University, Shanghai; 200234, China |
推荐引用方式 GB/T 7714 | Dai, Jiawei,Pan, Yubai,Wang, Wei,et al. Fabrication of Tb3Al5O12transparent ceramics using co-precipitated nanopowders[J]. Optical Materials,2017,73:38-44. |
APA | Dai, Jiawei.,Pan, Yubai.,Wang, Wei.,Luo, Wei.,Xie, Tengfei.,...&Li, Jiang.(2017).Fabrication of Tb3Al5O12transparent ceramics using co-precipitated nanopowders.Optical Materials,73,38-44. |
MLA | Dai, Jiawei,et al."Fabrication of Tb3Al5O12transparent ceramics using co-precipitated nanopowders".Optical Materials 73(2017):38-44. |
入库方式: OAI收割
来源:上海硅酸盐研究所
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