中国科学院机构知识库网格
Chinese Academy of Sciences Institutional Repositories Grid
Anionic SO3H-functionalized ionic liquid: An efficient and recyclable catalyst for the Pechmann reaction of phenols with ethyl acetoacetate

文献类型:期刊论文

作者Song DY(宋大勇)1,2; Liang YM(梁永民); Liang YM(梁永民)1; Chen J(陈静)2
刊名Synthetic Communications
出版日期2018
卷号48期号:6页码:692-698
关键词Anionic So3h-functionalized Coumarins Ionic Liquid Pechmann Reaction
ISSN号0039-7911
DOI10.1080/00397911.2017.1418000
英文摘要

This paper has reported an anionic SO3H-functionalized ionic liquid N-methylimidazolium sulfomethylsulfonate ([Hmim][HO3SCH2SO3]) for the synthesis of coumarins by Pechmann reaction. The [Hmim][HO3SCH2SO3] is easier to prepare by one-step neutralization reaction of N-methylimidazole with methanedisulfonic acid and show high catalytic performance for Pechmann reaction. Besides, the catalyst can simply be separated from the reaction mixture and recycled ten times without noticeable loss of activity.

学科主题物理化学与绿色催化
资助项目分子催化与技术研究组
语种英语
WOS记录号WOS:000426955600011
资助机构the National Natural Science Foundation of China (Project No. 21473225)
源URL[http://210.77.64.217/handle/362003/23687]  
专题兰州化学物理研究所_OSSO国家重点实验室
通讯作者Liang YM(梁永民)
作者单位1.Lanzhou Univ, State Key Lab Appl Organ Chem, Lanzhou, Gansu, Peoples R China
2.Chinese Acad Sci, Lanzhou Inst Chem Phys, State Key Lab Oxo Synth & Select Oxidat, Lanzhou, Gansu, Peoples R China
推荐引用方式
GB/T 7714
Song DY,Liang YM,Liang YM,et al. Anionic SO3H-functionalized ionic liquid: An efficient and recyclable catalyst for the Pechmann reaction of phenols with ethyl acetoacetate[J]. Synthetic Communications,2018,48(6):692-698.
APA Song DY,梁永民,Liang YM,&Chen J.(2018).Anionic SO3H-functionalized ionic liquid: An efficient and recyclable catalyst for the Pechmann reaction of phenols with ethyl acetoacetate.Synthetic Communications,48(6),692-698.
MLA Song DY,et al."Anionic SO3H-functionalized ionic liquid: An efficient and recyclable catalyst for the Pechmann reaction of phenols with ethyl acetoacetate".Synthetic Communications 48.6(2018):692-698.

入库方式: OAI收割

来源:兰州化学物理研究所

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