Fast analysis of capillary electrochromatography with non-porous ODS as the stationary phase
文献类型:期刊论文
作者 | Zhang, LH; Zhang, YK; Zhu, J; Zou, HF |
刊名 | analytical letters
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出版日期 | 1999 |
卷号 | 32期号:13页码:2679-2690 |
关键词 | capillary electrochromatography fast analysis non-porous ODS aromatic compounds DNPH derived aldehydes and ketones |
英文摘要 | high-speed capillary electrochromatography was developed on both short and long packed columns with 2 mu m non-porous ods as the stationary phase. factors that affect the analysis time of samples, such as voltage, electrolyte concentration, ph and organic modifier concentration in the mobile phase, were studied systematically. fast analysis of aromatic compounds within 13 seconds was realized with column efficiency of 573,000 plates/m and a r.s.d.% of the retention times of all components in 8 consecutive injections below 1.0%. which demonstrated the high efficiency and high reproducibility of such a technique. in addition, dnph derived aldehydes and ketones in both standards and environmental samples were separated with high speed. |
WOS标题词 | science & technology ; physical sciences |
类目[WOS] | chemistry, analytical |
研究领域[WOS] | chemistry |
关键词[WOS] | liquid-chromatography ; electrophoresis ; separation |
收录类别 | SCI |
原文出处 | true |
语种 | 英语 |
WOS记录号 | WOS:000083212300012 |
公开日期 | 2010-11-30 |
源URL | [http://159.226.238.44/handle/321008/85555] ![]() |
专题 | 大连化学物理研究所_中国科学院大连化学物理研究所 |
作者单位 | Chinese Acad Sci, Dalian Inst Chem Phys, Natl Chromatog R&A Ctr, Dalian 116011, Peoples R China |
推荐引用方式 GB/T 7714 | Zhang, LH,Zhang, YK,Zhu, J,et al. Fast analysis of capillary electrochromatography with non-porous ODS as the stationary phase[J]. analytical letters,1999,32(13):2679-2690. |
APA | Zhang, LH,Zhang, YK,Zhu, J,&Zou, HF.(1999).Fast analysis of capillary electrochromatography with non-porous ODS as the stationary phase.analytical letters,32(13),2679-2690. |
MLA | Zhang, LH,et al."Fast analysis of capillary electrochromatography with non-porous ODS as the stationary phase".analytical letters 32.13(1999):2679-2690. |
入库方式: OAI收割
来源:大连化学物理研究所
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