New method for analysis of Chinese herbal complex prescription and its application
文献类型:期刊论文
作者 | Xiao, HB; Liang, XM; Lu, PZ; Chan, CK |
刊名 | chinese science bulletin
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出版日期 | 1999-07-01 |
卷号 | 44期号:13页码:1164-1172 |
关键词 | Chinese herbal complex prescription black box analysis HPLC unified method Dang-Gui-Bu-Xue-Tang |
英文摘要 | traditional chinese medicine (tcm) is a great treasure of china, the analysis of which is an arduous task. the viewpoint that all chemical constituents of chinese herbal complex prescription should be analyzed as a black box is elucidated for the first time. intelligent multi-mode multi-column chromatographic system (immcc) with its hybrids is the basic method and hplc unified method is the breakthrough for the black box analysis. dang-gui-bu-xue-tang was selected as a typical tcm and a systematic separation method from non-aqueous mobile phase to pure water mobile phase was put forward in order to convert unknown sample to known sample. the a, c values and uv spectra of 66 components of astragalus, 78 components of angelica and 71 components of dang-gui-bu-xue-tang were obtained. intelligent optimization and peak identification method and software for complex samples were developed and the optimum multi-step multi-binary gradient curve of mobile phase for astragalus was ascertained. the maximum error and minimum error of predicted retention time for all components of astragalus are 8.62% and 0.05% respectively. all components of astragalus were compared with those of angelica and it is found that many components of astragalus are the same as those of angelica, while the contents of these components are different. many components of dang-gui-bu-xue-tang are also the same as those of astragalus and angelica with different contents. |
WOS标题词 | science & technology |
类目[WOS] | multidisciplinary sciences |
研究领域[WOS] | science & technology - other topics |
收录类别 | SCI |
原文出处 | true |
语种 | 英语 |
WOS记录号 | WOS:000082955000003 |
公开日期 | 2010-11-30 |
源URL | [http://159.226.238.44/handle/321008/86109] ![]() |
专题 | 大连化学物理研究所_中国科学院大连化学物理研究所 |
作者单位 | 1.Chinese Acad Sci, Dalian Inst Chem Phys, Dalian 116012, Peoples R China 2.Govt Lab, Hong Kong, Hong Kong |
推荐引用方式 GB/T 7714 | Xiao, HB,Liang, XM,Lu, PZ,et al. New method for analysis of Chinese herbal complex prescription and its application[J]. chinese science bulletin,1999,44(13):1164-1172. |
APA | Xiao, HB,Liang, XM,Lu, PZ,&Chan, CK.(1999).New method for analysis of Chinese herbal complex prescription and its application.chinese science bulletin,44(13),1164-1172. |
MLA | Xiao, HB,et al."New method for analysis of Chinese herbal complex prescription and its application".chinese science bulletin 44.13(1999):1164-1172. |
入库方式: OAI收割
来源:大连化学物理研究所
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