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Magnetic "one-step" quick, easy, cheap, effective, rugged and safe method for the fast determination of pesticide residues in freshly squeezed juice
文献类型：期刊论文
| 作者 | Feng, Yu-Qi2; Yuan, Bi-Feng2; Yu, Qiong-Wei2; Zheng, Shu-Jian2; Ding, Jun1; Zheng, Hao-Bo2 |
| 刊名 | JOURNAL OF CHROMATOGRAPHY A
 |
| 出版日期 | 2015-06-12 |
| 卷号 | 1398页码:1-10 |
| 关键词 | QuEChERS Pesticide residue Magnetic adsorbent Gas chromatography-mass spectrometry Freshly squeezed juice |
| ISSN号 | 0021-9673 |
| DOI | 10.1016/j.chroma.2015.04.021 |
| 英文摘要 | A "one-step" quick, easy, cheap, effective, rugged and safe (QuEChERS) method was proposed for pesticide residue analysis in freshly squeezed juice of fruits and vegetables. In this method, a new magnetic adsorbent prepared by simple physical blending was adopt, which could endow the sample mixture with magnetic separability. To achieve the best performance of the modified QuEChERS towards target analytes, the amounts of adsorbents were investigated. Under the optimized conditions, a simple, rapid and sensitive method for the determination of 11 pesticide residues in freshly squeezed juice was established by coupling modified QuEChERS to gas chromatography/mass spectrometry analysis. The limits of quantification of the proposed method for 11 pesticides ranged from 2.0 to 49.6 ng/g. Good linearities (R value >= 0.9993) were achieved at different concentration ranges, and acceptable method reproducibility was obtained by evaluating intra- and inter-day precisions with the relative standard deviations being less than 8.5% and 13.5%, respectively. The recoveries were in the range of 70.3-114.1% at different concentrations for real samples. Compared with the traditional QuEChERS methods, extraction/partitioning and purification were integrated into one step in the proposed method, which thus was time-saving (within 3.5 min) with keeping good clean-up performance. (C) 2015 Elsevier B.V. All rights reserved. |
| 资助项目 | National Natural Science Foundation of China[91017013] ; National Natural Science Foundation of China[91217309] ; Fundamental Research Funds for the Central Universities |
| WOS研究方向 | Biochemistry & Molecular Biology ; Chemistry |
| 语种 | 英语 |
| WOS记录号 | WOS:000355054300001 |
| 出版者 | ELSEVIER SCIENCE BV |
| 源URL | [http://202.127.146.157/handle/2RYDP1HH/249]  |
| 专题 | 中国科学院武汉植物园 |
| 通讯作者 | Feng, Yu-Qi |
| 作者单位 | 1.Chinese Acad Sci, Key Lab Plant Germplasm Enhancement & Specialty A, Wuhan Bot Garden, Wuhan 430074, Peoples R China 2.Wuhan Univ, Dept Chem, Key Lab Analyt Chem Biol & Med, Minist Educ, Wuhan 430072, Peoples R China |
| 推荐引用方式 GB/T 7714 | Feng, Yu-Qi,Yuan, Bi-Feng,Yu, Qiong-Wei,et al. Magnetic "one-step" quick, easy, cheap, effective, rugged and safe method for the fast determination of pesticide residues in freshly squeezed juice[J]. JOURNAL OF CHROMATOGRAPHY A,2015,1398:1-10. |
| APA | Feng, Yu-Qi,Yuan, Bi-Feng,Yu, Qiong-Wei,Zheng, Shu-Jian,Ding, Jun,&Zheng, Hao-Bo.(2015).Magnetic "one-step" quick, easy, cheap, effective, rugged and safe method for the fast determination of pesticide residues in freshly squeezed juice.JOURNAL OF CHROMATOGRAPHY A,1398,1-10. |
| MLA | Feng, Yu-Qi,et al."Magnetic "one-step" quick, easy, cheap, effective, rugged and safe method for the fast determination of pesticide residues in freshly squeezed juice".JOURNAL OF CHROMATOGRAPHY A 1398(2015):1-10. |
入库方式： OAI收割
来源：武汉植物园
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