Column switching-back flushing technique for the analysis of aromatic compounds in gasoline
文献类型：期刊论文
| 作者 | Wang, HW; Xu, H; Guan, YF |
| 刊名 | journal of chromatography a
 |
| 出版日期 | 2002-10-04 |
| 卷号 | 972期号:2页码:253-258 |
| 关键词 | column switching gasoline instrumentation hydrocarbons aromatic |
| 英文摘要 | a simple method, based on the technique of capillary column switching-back flushing, has been developed for the detailed analysis of aromatic compounds in gasoline. the sample was first separated on a 30-m long ov-2330 polar precolumn and then backflushed onto a nonpolar analytical column. the early eluting components from the precolumn and the components of interest (aromatic compounds plus heavier compounds) eluting from the analytical column are all directed to the same flame ionization detection system through a t piece, which permits the quantitative analysis of aromatic hydrocarbons in gasoline by a normalization method using correcting factors. the switching time window of the method is +/-5 s, resulting in easier operation and higher reliability. the reproducibility of the quantitative analysis was less than or equal to3% rsd for real gasoline samples. (c) 2002 elsevier science b.v. all rights reserved. |
| WOS标题词 | science & technology ; life sciences & biomedicine ; physical sciences |
| 类目[WOS] | biochemical research methods ; chemistry, analytical |
| 研究领域[WOS] | biochemistry & molecular biology ; chemistry |
| 关键词[WOS] | chromatographic pna analysis ; hydrocarbon-type samples ; gas-chromatography |
| 收录类别 | SCI |
| 原文出处 | true |
| 语种 | 英语 |
| WOS记录号 | WOS:000178367700011 |
| 公开日期 | 2010-11-30 |
| 源URL | [http://159.226.238.44/handle/321008/91443]  |
| 专题 | 大连化学物理研究所_中国科学院大连化学物理研究所 |
| 作者单位 | Chinese Acad Sci, Dalian Inst Chem Phys, Dept Analyt Chem & Micro Instrumentat, Dalian 116012, Peoples R China |
| 推荐引用方式 GB/T 7714 | Wang, HW,Xu, H,Guan, YF. Column switching-back flushing technique for the analysis of aromatic compounds in gasoline[J]. journal of chromatography a,2002,972(2):253-258. |
| APA | Wang, HW,Xu, H,&Guan, YF.(2002).Column switching-back flushing technique for the analysis of aromatic compounds in gasoline.journal of chromatography a,972(2),253-258. |
| MLA | Wang, HW,et al."Column switching-back flushing technique for the analysis of aromatic compounds in gasoline".journal of chromatography a 972.2(2002):253-258. |
入库方式： OAI收割
来源：大连化学物理研究所
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