Quantitative determination of compounds in tobacco essential oils by comprehensive two-dimensional gas chromatography coupled to time-of-flight mass spectrometry
文献类型:期刊论文
作者 | Zhu, SK; Lu, X; Dong, L; Xing, J; Su, XL; Kong, HW; Xu, GW; Wu, CY |
刊名 | journal of chromatography a
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出版日期 | 2005-09-09 |
卷号 | 1086期号:1-2页码:107-114 |
关键词 | comprehensive two-dimensional gas chromatography time-of-flight mass spectrometry gas chromatography-mass spectrometry multiple internal standards calibration essential oils tobacco |
产权排序 | 2;2 |
通讯作者 | 吴采樱 |
英文摘要 | a quantitative analysis of the individual compounds in tobacco essential oils is performed by comprehensive two-dimensional gas chromatography (gc x gc) combined with flame ionization detector (fid). a time-of-flight mass spectrometer (tof/ms) was coupled to gc x gc for the identification of the resolved peaks. the response of a flame ionization detector to different compound classes was calibrated using multiple internal standards. in total, 172 compounds were identified with good match and 61 compounds with high probability value were reliably quantified. for comparative purposes, the essential oil sample was also quantified by one-dimensional gas chromatography-mass spectrometry (gc/ms) with multiple internal standards method. the results showed that there was close agreement between the two analysis methods when the peak purity and match quality in one-dimensional gc/ms are high enough. (c) 2005 elsevier b.v. all rights reserved. |
WOS标题词 | science & technology ; life sciences & biomedicine ; physical sciences |
类目[WOS] | biochemical research methods ; chemistry, analytical |
研究领域[WOS] | biochemistry & molecular biology ; chemistry |
关键词[WOS] | cigarette-smoke |
收录类别 | ISTP ; SCI |
原文出处 | true |
语种 | 英语 |
WOS记录号 | WOS:000231185500012 |
公开日期 | 2010-11-30 |
源URL | [http://159.226.238.44/handle/321008/92903] ![]() |
专题 | 大连化学物理研究所_中国科学院大连化学物理研究所 |
作者单位 | 1.Wuhan Univ, Coll Chem & Mol Sci, Wuhan 430072, Peoples R China 2.Chinese Acad Sci, Dalian Inst Chem Phys, Natl Chromatog R&A Ctr, Dalian 116011, Peoples R China |
推荐引用方式 GB/T 7714 | Zhu, SK,Lu, X,Dong, L,et al. Quantitative determination of compounds in tobacco essential oils by comprehensive two-dimensional gas chromatography coupled to time-of-flight mass spectrometry[J]. journal of chromatography a,2005,1086(1-2):107-114. |
APA | Zhu, SK.,Lu, X.,Dong, L.,Xing, J.,Su, XL.,...&Wu, CY.(2005).Quantitative determination of compounds in tobacco essential oils by comprehensive two-dimensional gas chromatography coupled to time-of-flight mass spectrometry.journal of chromatography a,1086(1-2),107-114. |
MLA | Zhu, SK,et al."Quantitative determination of compounds in tobacco essential oils by comprehensive two-dimensional gas chromatography coupled to time-of-flight mass spectrometry".journal of chromatography a 1086.1-2(2005):107-114. |
入库方式: OAI收割
来源:大连化学物理研究所
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